1EEA
Acetylcholinesterase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Temperature [K] | 298 |
Detector technology | AREA DETECTOR |
Collection date | 1987-01-15 |
Detector | XENTRONICS |
Spacegroup name | F 2 2 2 |
Unit cell lengths | 140.860, 201.460, 235.770 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | ? - 4.500 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2ace |
Data reduction software | X-GEN |
Data scaling software | X-GEN |
Phasing software | X-PLOR |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 34.300 | 4.650 |
High resolution limit [Å] | 4.500 | 4.500 |
Rmerge | 0.097 | 0.272 |
Number of reflections | 9717 | |
<I/σ(I)> | 6.7 | 2 |
Completeness [%] | 95.3 | 75.2 |
Redundancy | 3.2 | 1.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8 | pH 8.0 |