1DVJ
CRYSTAL STRUCTURE OF OROTIDINE MONOPHOSPHATE DECARBOXYLASE COMPLEXED WITH 6-AZAUMP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS |
Synchrotron site | APS |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 1999-06-15 |
Detector | ADSC QUANTUM 4 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 72.950, 98.620, 73.250 |
Unit cell angles | 90.00, 104.03, 90.00 |
Refinement procedure
Resolution | 30.000 - 1.500 |
R-factor | 0.174 |
Rwork | 0.174 |
R-free | 0.18800 |
RMSD bond length | 0.015 |
RMSD bond angle | 1.700 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | CNS (0.5) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 1.580 |
High resolution limit [Å] | 1.500 | 1.500 |
Rmerge | 0.058 | 0.326 |
Total number of observations | 1127371 * | |
Number of reflections | 156498 | |
<I/σ(I)> | 8.9 | |
Completeness [%] | 97.6 | 87.9 |
Redundancy | 7.2 | 6.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 6.5 | 298 | unpublished data * |