1DU3
Crystal structure of TRAIL-SDR5
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PHOTON FACTORY BEAMLINE BL-6A |
| Synchrotron site | Photon Factory |
| Beamline | BL-6A |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 1999-01-01 |
| Detector | FUJI |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 68.630, 124.810, 128.370 |
| Unit cell angles | 90.00, 104.49, 90.00 |
Refinement procedure
| Resolution | 8.000 - 2.200 |
| R-factor | 0.212 |
| Rwork | 0.291 |
| R-free | 0.29100 |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.772 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | AMoRE |
| Refinement software | X-PLOR (3.851) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.000 | 2.280 |
| High resolution limit [Å] | 2.200 | 2.200 |
| Rmerge | 0.061 | 0.306 |
| Number of reflections | 93618 | |
| <I/σ(I)> | 12 | |
| Completeness [%] | 93.1 * | 70 |
| Redundancy | 3.7 | 2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | unknown * | 4.5 * | 295 | PEG 1000, Sodium Acetate, Sodium Chloride, pH 4.6, EVAPORATION, temperature 22K |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | 1 | PEG3000 | 16 (%) | |
| 2 | 1 | 1 | sodium acetate | 0.6 (M) | |
| 3 | 1 | 1 | 0.6 (M) |
