1DU3
Crystal structure of TRAIL-SDR5
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-6A |
Synchrotron site | Photon Factory |
Beamline | BL-6A |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 1999-01-01 |
Detector | FUJI |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 68.630, 124.810, 128.370 |
Unit cell angles | 90.00, 104.49, 90.00 |
Refinement procedure
Resolution | 8.000 - 2.200 |
R-factor | 0.212 |
Rwork | 0.291 |
R-free | 0.29100 |
RMSD bond length | 0.011 |
RMSD bond angle | 1.772 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | X-PLOR (3.851) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.280 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.061 | 0.306 |
Number of reflections | 93618 | |
<I/σ(I)> | 12 | |
Completeness [%] | 93.1 * | 70 |
Redundancy | 3.7 | 2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 4.5 * | 295 | PEG 1000, Sodium Acetate, Sodium Chloride, pH 4.6, EVAPORATION, temperature 22K |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | PEG3000 | 16 (%) | |
2 | 1 | 1 | sodium acetate | 0.6 (M) | |
3 | 1 | 1 | 0.6 (M) |