1DST
MUTANT OF FACTOR D WITH ENHANCED CATALYTIC ACTIVITY
Experimental procedure
Temperature [K] | 295 |
Detector technology | AREA DETECTOR |
Detector | SIEMENS |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 45.380, 45.380, 175.210 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 7.500 - 2.000 |
R-factor | 0.198 * |
R-free | 0.21300 |
RMSD bond length | 0.020 |
RMSD bond angle | 0.035 |
Data reduction software | XENGEN |
Data scaling software | XENGEN |
Refinement software | PROLSQ |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 20.000 |
High resolution limit [Å] | 2.000 |
Rmerge | 0.076 |
Total number of observations | 59734 * |
Number of reflections | 13899 * |
Completeness [%] | 94.0 |
Redundancy | 6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion * | 6.8 | 22 * | pH 6.8 |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | MES | 50 (mM) | |
2 | 1 | reservoir | PEG6000 |