1DNP
STRUCTURE OF DEOXYRIBODIPYRIMIDINE PHOTOLYASE
Experimental procedure
Source type | ROTATING ANODE |
Detector technology | AREA DETECTOR |
Collection date | 1991-10 |
Detector | XUONG-HAMLIN MULTIWIRE |
Spacegroup name | P 1 |
Unit cell lengths | 62.600, 72.200, 58.500 |
Unit cell angles | 99.10, 101.50, 72.00 |
Refinement procedure
Resolution | 10.000 - 2.300 |
R-factor | 0.172 |
Rwork | 0.172 |
R-free | 0.24600 |
RMSD bond length | 0.012 |
RMSD bond angle | 1.390 * |
Data reduction software | XDS |
Phasing software | X-PLOR (3.1) |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | |
High resolution limit [Å] | 2.300 |
Rmerge | 0.043 |
Total number of observations | 76311 * |
Number of reflections | 33086 |
Completeness [%] | 78.3 |
Redundancy | 2.45 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion * | 7.6 * | seeding. refer to Park, H.W., (1993) J.Mol.Biol., 231, 1122. * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | photolyase | 4 (mg/ml) | |
2 | 1 | drop | glycerol | 20 (%) | |
3 | 1 | drop | Tris-HCl | 50 (mM) | |
4 | 1 | drop | reservoir | ||
5 | 1 | reservoir | PEG4000 | 30 (%(w/v)) | |
6 | 1 | reservoir | 0.9 (M) | ||
7 | 1 | reservoir | Tris-HCl | 100 (mM) |