1DKS
CKSHS1: HUMAN CYCLIN DEPENDENT KINASE SUBUNIT, TYPE 1 IN COMPLEX WITH PHOSPHATE
Experimental procedure
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 295 |
Detector technology | AREA DETECTOR |
Detector | SIEMENS-NICOLET X100 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 94.000, 94.000, 137.400 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 6.000 - 3.200 |
R-factor | 0.183 |
Rwork | 0.183 |
R-free | 0.29000 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.900 |
Data reduction software | XDS |
Phasing software | X-PLOR (3.1) |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 3.300 |
High resolution limit [Å] | 3.200 | 3.200 |
Rmerge | 0.093 * | 0.270 |
Number of reflections | 5692 | |
<I/σ(I)> | 25 | 4 |
Completeness [%] | 97.0 | 85 |
Redundancy | 8 * | 2. * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion * | 7.4 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | ammonium phosphate | 5 (%(v/v)) | from a 3.5 M stock solution |
2 | 1 | reservoir | PEG4000 | 25 (%) |