1DFP
FACTOR D INHIBITED BY DIISOPROPYL FLUOROPHOSPHATE
Experimental procedure
Source type | ROTATING ANODE |
Source details | RIGAKU RUH2R |
Temperature [K] | 293 |
Detector technology | CCD |
Collection date | 1995-02 |
Detector | SIEMENS X1000 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 40.600, 125.700, 41.900 |
Unit cell angles | 90.00, 110.05, 90.00 |
Refinement procedure
Resolution | 8.000 - 2.400 |
R-factor | 0.148 |
Rwork | 0.148 |
R-free | 0.22800 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1dsu |
RMSD bond length | 0.011 |
RMSD bond angle | 27.100 * |
Data reduction software | XENGEN |
Data scaling software | XENGEN |
Phasing software | X-PLOR (3.1) |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 15.000 | 2.550 |
High resolution limit [Å] | 2.400 | 2.400 |
Rmerge | 0.053 | 0.120 |
Total number of observations | 64840 * | |
Number of reflections | 14663 | |
<I/σ(I)> | 23.2 | 4.6 |
Completeness [%] | 95.4 | 75 |
Redundancy | 4.4 | 2.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 5.8 | used to seeding * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | MES | 50 (mM) | |
2 | 1 | reservoir | PEG6000 | 12-16 (%) | |
3 | 1 | reservoir | 0.2 (M) |