1DBR

HYPOXANTHINE GUANINE XANTHINE

Experimental procedure

Spacegroup name	P 1 21 1
Unit cell lengths	65.150, 109.220, 79.740
Unit cell angles	90.00, 111.80, 90.00

Refinement procedure

Resolution	10.000 - 2.400
R-factor	0.156 *
Rwork	0.168
RMSD bond length	0.018 *
RMSD bond angle	2.540 *
Refinement software	TNT

Data quality characteristics

	Overall	Outer shell
High resolution limit [Å]	2.400 *	2.400 *
Rmerge	0.065 *
Total number of observations	67476 *
Number of reflections	37403 *
Completeness [%]	90.0 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *	8.45 *	4 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	PEG4000	13 (%)
2	1	reservoir		0.2 (M)
3	1	reservoir	Tris-HCl	0.1 (M)