1D2E
CRYSTAL STRUCTURE OF MITOCHONDRIAL EF-TU IN COMPLEX WITH GDP
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ELETTRA BEAMLINE 5.2R |
| Synchrotron site | ELETTRA |
| Beamline | 5.2R |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 1998-03-08 |
| Detector | MARRESEARCH |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 59.090, 119.780, 128.890 |
| Unit cell angles | 90.00, 96.97, 90.00 |
Refinement procedure
| Resolution | 34.700 - 1.940 |
| R-factor | 0.237 |
| Rwork | 0.237 |
| R-free | 0.25700 |
| RMSD bond length | 0.007 |
| RMSD bond angle | 23.100 * |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | AMoRE |
| Refinement software | CNS (0.3) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 34.700 | 2.010 |
| High resolution limit [Å] | 1.940 | 1.940 |
| Rmerge | 0.048 | 0.334 |
| Number of reflections | 128896 | |
| <I/σ(I)> | 17.6 | |
| Completeness [%] | 98.2 | 98 |
| Redundancy | 3 | 2.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | unknown * | 7.2 | 277 | MME 2K, pH 7.2, VAPOR DIFFUSION, SITTING DROP, temperature 4K |
