1CWD
HUMAN P56LCK TYROSINE KINASE COMPLEXED WITH PHOSPHOPEPTIDE
Experimental procedure
Spacegroup name | P 21 21 21 |
Unit cell lengths | 44.660, 46.660, 58.298 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 8.000 - 2.250 |
R-factor | 0.185 |
Rwork | 0.185 |
RMSD bond length | 0.015 |
RMSD bond angle | 1.850 |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 8.000 |
High resolution limit [Å] | 2.250 |
Rmerge | 0.077 * |
Total number of observations | 13232 * |
Number of reflections | 5072 * |
Completeness [%] | 95.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 5.05 * | 22 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | 10 (mM) | ||
2 | 1 | drop | PEG8000 | 10.5 (%(w/v)) | |
3 | 1 | drop | 0.02 (%(w/v)) | ||
4 | 1 | drop | Lck/peptide 1 | 2 (mM) | |
5 | 1 | reservoir | 20 (mM) | ||
6 | 1 | reservoir | PEG8000 | 21 (%(w/v)) | |
7 | 1 | reservoir | 0.04 (%(w/v)) |