1CT8
CATALYTIC ANTIBODY 7C8 COMPLEX
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | LURE BEAMLINE DW32 |
Synchrotron site | LURE |
Beamline | DW32 |
Temperature [K] | 278 |
Detector technology | IMAGE PLATE |
Collection date | 1997-04-08 |
Detector | MARRESEARCH |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 54.558, 65.612, 117.761 |
Unit cell angles | 90.00, 95.56, 90.00 |
Refinement procedure
Resolution | 14.300 - 2.200 |
R-factor | 0.211 * |
Rwork | 0.211 |
R-free | 0.27500 |
RMSD bond length | 0.011 |
RMSD bond angle | 1.750 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | X-PLOR (3.843) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 14.300 | 2.280 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.066 | 0.253 |
Total number of observations | 98277 * | |
Number of reflections | 40238 | |
<I/σ(I)> | 15.2 | |
Completeness [%] | 97.9 | 95.7 |
Redundancy | 2.44 | 2.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 4 | 291 | used macroseeding * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | Fab | 5 (mg/ml) | |
2 | 1 | 1 | 150 (mM) | ||
3 | 1 | 2 | PEG1000 | 22-26 (%(w/v)) | |
4 | 1 | 2 | ammonium sulfate | 0.2 (M) |