1CS8
CRYSTAL STRUCTURE OF PROCATHEPSIN L
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | CHESS BEAMLINE A1 |
| Synchrotron site | CHESS |
| Beamline | A1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 1996-02-13 |
| Detector | ADSC |
| Spacegroup name | P 32 2 1 |
| Unit cell lengths | 104.290, 104.290, 85.990 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 8.000 - 1.800 |
| Rwork | 0.207 |
| R-free | 0.22850 |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.375 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | AMoRE |
| Refinement software | X-PLOR (3.843) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 45.000 | 1.860 |
| High resolution limit [Å] | 1.800 | 1.800 |
| Rmerge | 0.044 | 0.224 |
| Number of reflections | 47257 | |
| Completeness [%] | 93.9 | 66.7 |
| Redundancy | 3.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | MICROBATCH | 7.8 | 293.2 | Na,K,Phosphate, pH 7.8, MICROBATCH, temperature 20.2K |
