1COF
YEAST COFILIN, ORTHORHOMBIC CRYSTAL FORM
Experimental procedure
Source type | ROTATING ANODE |
Source details | RIGAKU RUH2R |
Temperature [K] | 290 |
Detector technology | AREA DETECTOR |
Collection date | 1995 |
Detector | SIEMENS |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 30.669, 48.773, 101.367 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 8.000 - 2.300 |
Rwork | 0.184 |
Structure solution method | MIR |
RMSD bond length | 0.011 * |
RMSD bond angle | 1.610 * |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASES |
Refinement software | PROFFT |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 26.200 |
High resolution limit [Å] | 2.300 |
Rmerge | 0.067 * |
Number of reflections | 6330 |
<I/σ(I)> | 18.5 |
Completeness [%] | 87.5 |
Redundancy | 2.33 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 7.2 | CRYSTALLIZED FROM 25% PEG 4000 SOLUTION., pH 7.2 |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | PEG4000 | 20-30 (%) |