1CD9
2:2 COMPLEX OF G-CSF WITH ITS RECEPTOR
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL41XU |
Synchrotron site | SPring-8 |
Beamline | BL41XU |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 1999-06-15 |
Detector | RIGAKU |
Spacegroup name | I 41 2 2 |
Unit cell lengths | 125.467, 125.467, 372.771 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 25.000 * - 2.800 |
Rwork | 0.237 |
R-free | 0.29800 * |
Structure solution method | MIRAS |
RMSD bond length | 0.012 |
RMSD bond angle | 0.033 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | MLPHARE |
Refinement software | REFMAC |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 2.800 |
Rmerge | 0.057 |
Total number of observations | 169036 * |
Number of reflections | 35565 |
Completeness [%] | 95.4 |
Redundancy | 4.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 7.5 | manuscript in preparation * |