1CBY

DELTA-ENDOTOXIN

Experimental procedure

Source type	SYNCHROTRON
Source details	SRS BEAMLINE PX9.6
Synchrotron site	SRS
Beamline	PX9.6
Temperature [K]	293
Detector technology	IMAGE PLATE
Collection date	1993-10-25
Detector	MARRESEARCH
Spacegroup name	P 61 2 2
Unit cell lengths	66.810, 66.810, 170.790
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	19.000 - 2.600
R-factor	0.197
Rwork	0.197
R-free	0.26100
RMSD bond length	0.005
RMSD bond angle	24.140 *
Data reduction software	MOSFLM
Phasing software	X-PLOR (3.1)
Refinement software	X-PLOR (3.1)

Data quality characteristics

	Overall
Low resolution limit [Å]	19.000
High resolution limit [Å]	2.600
Rmerge	0.071
Number of reflections	7235
Completeness [%]	96.2
Redundancy	5.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Microdialysis *	8.5 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	Tris-HCl	100 (mM)
2	1	reservoir	urea	50 (mM)