1BRU

STRUCTURE OF PORCINE PANCREATIC ELASTASE COMPLEXED WITH THE ELASTASE INHIBITOR GR143783

Experimental procedure

Source type	ROTATING ANODE
Source details	ELLIOTT GX-21
Temperature [K]	287
Detector technology	DIFFRACTOMETER
Collection date	1992-10
Detector	ENRAF-NONIUS FAST
Spacegroup name	P 21 21 21
Unit cell lengths	41.590, 46.450, 128.230
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	8.000 - 2.300
R-factor	0.147
Rwork	0.147
RMSD bond length	0.014
RMSD bond angle	2.700
Data reduction software	MADNESS
Refinement software	X-PLOR

Data quality characteristics

	Overall
Low resolution limit [Å]	20.000
High resolution limit [Å]	2.300
Rmerge	0.067
Number of reflections	8677
Completeness [%]	95.0
Redundancy	2.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1		5		pH 5.0