1BMA

BENZYL METHYL AMINIMIDE INHIBITOR COMPLEXED TO PORCINE PANCREATIC ELASTASE

Experimental procedure

Collection date	1994-05-20
Detector	SIEMENS
Wavelength(s)	1.5148
Spacegroup name	P 21 21 21
Unit cell lengths	52.160, 57.680, 75.520
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	10.000 - 1.800
R-factor	0.192
Rwork	0.192
RMSD bond length	0.015
RMSD bond angle	26.800 *
Data reduction software	XDS
Data scaling software	XDS
Phasing software	X-PLOR (3.1)
Refinement software	X-PLOR (3.1)

Data quality characteristics

	Overall
Low resolution limit [Å]	10.000
High resolution limit [Å]	1.800
Rmerge	0.063
Total number of observations	44505 *
Number of reflections	39545
Completeness [%]	58.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *	5 *	2 *	or 20 degrees centigrade *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1	elastase	20 (mg/ml)
2	1	1	sodium sulfate	10 (mM)
3	1	2	sodium sulfate	1 (M)