1BHG
HUMAN BETA-GLUCURONIDASE AT 2.6 A RESOLUTION
Experimental procedure
Detector technology | AREA DETECTOR |
Collection date | 1993-02-10 |
Detector | XUONG-HAMLIN MULTIWIRE |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 95.100, 124.400, 134.500 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 7.000 - 2.530 |
R-factor | 0.231 |
Rwork | 0.231 |
R-free | 0.31000 |
RMSD bond length | 0.012 |
RMSD bond angle | 1.900 |
Data reduction software | XENGEN ((ANDERSON) |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 20.000 * |
High resolution limit [Å] | 2.600 * |
Rmerge | 0.078 |
Number of reflections | 46839 |
Completeness [%] | 93.2 |
Redundancy | 4.71 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion * | 7.5 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 2.1 (mg/ml) | |
2 | 1 | drop | MPD | 15 (%) | |
3 | 1 | drop | Tris-HCl | 5 (mM) | |
4 | 1 | drop | sodium azide | 0.01 (%(w/v)) | |
5 | 1 | reservoir | MPD | 30 (%) |