1BCF

THE STRUCTURE OF A UNIQUE, TWO-FOLD SYMMETRIC, HAEM-BINDING SITE

Experimental procedure

Spacegroup name	P 42 21 2
Unit cell lengths	211.100, 211.100, 145.200
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	8.000 - 2.900
R-factor	0.208
Rwork	0.208
RMSD bond length	0.016
RMSD bond angle	1.810
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall
High resolution limit [Å]	2.900 *
Rmerge	0.082 *
Total number of observations	733629 *
Number of reflections	71796 *
Completeness [%]	98.4 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Microdialysis *			Smith, J.M.A. (1989) J. Mol. Biol., 205, 465. *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1	ammonium sulfate	2 (M)
2	1	1		0.1 (M)