1AUJ
BOVINE TRYPSIN COMPLEXED TO META-CYANO-BENZYLIC INHIBITOR
Experimental procedure
Source type | ROTATING ANODE |
Source details | RIGAKU RUH2R |
Temperature [K] | 273 |
Detector technology | IMAGE PLATE |
Collection date | 1995-09 |
Detector | RIGAKU |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 55.000, 58.400, 67.600 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 8.000 - 2.100 |
R-factor | 0.169 |
Rwork | 0.169 |
Structure solution method | DIFFERENCE |
RMSD bond length | 0.011 |
RMSD bond angle | 1.900 |
Data reduction software | R-AXIS (SOFTWARE) |
Data scaling software | R-AXIS |
Phasing software | X-PLOR (3.1) |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | |
High resolution limit [Å] | 2.100 |
Rmerge | 0.052 * |
Completeness [%] | 90.0 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Batch method * | 7.5 * | Krieger, M., (1974) J. Mol. Biol., 83, 209. * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | 0.05 (M) | ||
2 | 1 | 1 | 1.25ml |