Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

1AHJ

NITRILE HYDRATASE

Experimental procedure
Source typeROTATING ANODE
Source detailsRIGAKU
Temperature [K]277
Detector technologyIMAGE PLATE
Collection date1996-09-09
DetectorMARRESEARCH
Spacegroup nameP 21 21 21
Unit cell lengths88.854, 144.239, 159.876
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution7.500 - 2.650
R-factor0.264
Rwork0.264
R-free0.28900
Structure solution methodMIRAS AVERAGING
RMSD bond length0.006
RMSD bond angle22.600

*

Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareSQUASH
Refinement softwareX-PLOR (3.1)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]30.0002.710
High resolution limit [Å]2.6502.650
Rmerge0.068

*

0.260

*

Total number of observations347098

*

Number of reflections56428
<I/σ(I)>20.33.2
Completeness [%]93.875.7
Redundancy6.2
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1Vapor diffusion, hanging drop

*

7

*

4

*

pH 8.5
Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
11dropenzyme10 (mg/ml)
21dropHEPES20 (mM)
31dropbutyrate40 (mM)
41reservoirPEG800027 (%)
51reservoir0.3 (M)
61reservoirTris0.1 (M)

217705

PDB entries from 2024-03-27

PDB statisticsPDBj update infoContact PDBjnumon