1A86

MMP8 WITH MALONIC AND ASPARTIC ACID BASED INHIBITOR

Experimental procedure

Temperature [K]	283
Collection date	1995-12
Spacegroup name	P 21 21 21
Unit cell lengths	33.140, 69.430, 72.620
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	6.000 * - 2.000
R-factor	0.183 *
Refinement software	X-PLOR

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	8.000 *
High resolution limit [Å]	1.900 *	1.900 *
Rmerge	0.056 *	0.272 *
Total number of observations	23574 *
Number of reflections	10905 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *	6 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein	1. (mg/ml)
2	1	drop	MES-NaOH	0.14 (M)
3	1	drop	inhibitor	15 (mM)
4	1	drop	PEG6000	5 (%(w/v))
5	1	reservoir	sodium phosphate	1 (M)