1A85
MMP8 WITH MALONIC AND ASPARAGINE BASED INHIBITOR
Experimental procedure
Temperature [K] | 283 |
Collection date | 1995-12 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 33.140, 69.430, 72.620 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 6.000 * - 2.000 |
R-factor | 0.188 * |
Refinement software | X-PLOR |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 6.500 * | |
High resolution limit [Å] | 1.800 * | 1.800 * |
Rmerge | 0.040 * | 0.215 * |
Total number of observations | 25225 * | |
Number of reflections | 14805 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 6 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 1. (mg/ml) | |
2 | 1 | drop | MES-NaOH | 0.14 (M) | |
3 | 1 | drop | inhibitor | 15 (mM) | |
4 | 1 | drop | PEG6000 | 5 (%(w/v)) | |
5 | 1 | reservoir | sodium phosphate | 1 (M) |