1A7Y
CRYSTAL STRUCTURE OF ACTINOMYCIN D
Experimental procedure
| Source type | ROTATING ANODE |
| Source details | SIEMENS |
| Temperature [K] | 133 |
| Detector technology | AREA DETECTOR |
| Collection date | 1997-11-03 |
| Detector | SIEMENS HI-STAR |
| Spacegroup name | P 1 |
| Unit cell lengths | 15.737, 15.887, 25.156 |
| Unit cell angles | 85.93, 86.19, 69.86 |
Refinement procedure
| Resolution | ? - 0.940 |
| R-factor | 0.058 |
| R-free | 0.06800 |
| Structure solution method | AB INITIO |
| RMSD bond length | 0.000 |
| RMSD bond angle | 0.000 |
| Data reduction software | SAINT |
| Data scaling software | SADABS |
| Phasing software | SHELXL-97 |
| Refinement software | SHELXL-97 |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 999.000 | 1.050 |
| High resolution limit [Å] | 0.940 | 0.940 |
| Rmerge | 0.044 | 0.072 |
| Total number of observations | 95014 * | |
| Number of reflections | 14126 | |
| <I/σ(I)> | 25.9 | 11.9 |
| Completeness [%] | 95.1 | 90.5 |
| Redundancy | 4.38 | 2.85 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | unknown * | 5 | PH 5.0 |
