1YQR
Catalytically inactive human 8-oxoguanine glycosylase crosslinked to oxoG containing DNA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Detector technology | IMAGE PLATE |
Collection date | 2002-12-20 |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.54 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 92.106, 92.106, 211.060 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 37.310 - 2.430 |
R-factor | 0.219 |
Rwork | 0.219 |
R-free | 0.25100 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.005 |
RMSD bond angle | 1.200 |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 37.310 | 2.520 |
High resolution limit [Å] | 2.430 | 2.430 |
Number of reflections | 19962 | |
Completeness [%] | 96.1 | 92.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |