1YA5
Crystal structure of the titin domains z1z2 in complex with telethonin
Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | EMBL/DESY, HAMBURG BEAMLINE X11 |
| Synchrotron site | EMBL/DESY, HAMBURG |
| Beamline | X11 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2001-12-06 |
| Detector | MARRESEARCH |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 46.326, 63.213, 242.584 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 14.920 - 2.445 |
| R-factor | 0.23278 |
| Rwork | 0.232 |
| R-free | 0.26496 |
| Structure solution method | MAD |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.370 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | MLPHARE |
| Refinement software | REFMAC (5.2) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 14.920 | 2.490 |
| High resolution limit [Å] | 2.445 | 2.445 |
| Rmerge | 0.053 | 0.395 |
| Number of reflections | 25248 | |
| <I/σ(I)> | 18.2 | 2.1 |
| Completeness [%] | 86.9 | |
| Redundancy | 3.3 | 3.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 4.45 | 298 | pH 4.45, VAPOR DIFFUSION, HANGING DROP, temperature 298K |
