1Y0H
Structure of Rv0793 from Mycobacterium tuberculosis
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ALS BEAMLINE 8.3.1 |
| Synchrotron site | ALS |
| Beamline | 8.3.1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2003-09-13 |
| Detector | ADSC QUANTUM 4 |
| Wavelength(s) | 0.979232 |
| Spacegroup name | P 1 |
| Unit cell lengths | 30.440, 34.600, 42.850 |
| Unit cell angles | 103.44, 107.96, 94.34 |
Refinement procedure
| Resolution | 29.590 - 1.600 |
| R-factor | 0.202 |
| Rwork | 0.173 |
| R-free | 0.21900 |
| Structure solution method | SAD |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.219 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | SOLVE (2.06) |
| Refinement software | REFMAC |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | 1.660 |
| High resolution limit [Å] | 1.600 | 1.600 |
| Rmerge | 0.098 | 0.485 |
| Number of reflections | 20461 | |
| <I/σ(I)> | 8.5 | 4.8 |
| Completeness [%] | 96.9 | 95.4 |
| Redundancy | 3.7 | 3.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7 | 295 | PEG20K, hepes, ammonium acetate, ethylene glycol, isopropanol, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 295K |
