1XR1
Crystal structure of hPim-1 kinase in complex with AMP-PNP at 2.1 A Resolution
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU300 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Detector | RIGAKU RAXIS IV |
Spacegroup name | P 65 |
Unit cell lengths | 96.680, 96.680, 80.020 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 29.430 - 2.100 |
Rwork | 0.267 |
R-free | 0.30100 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 1.200 |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | CNX (2002) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 29.400 |
High resolution limit [Å] | 1.700 |
Rmerge | 0.075 |
Number of reflections | 40217 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 298 | 30% PEG1500, 0.1 M Hepes pH 7.5, 0.3 M NaCl, VAPOR DIFFUSION, HANGING DROP, temperature 25K |