1XEJ
THE CRYSTAL STRUCTURES OF LYSOZYME AT VERY LOW LEVELS OF HYDRATION
Experimental procedure
Temperature [K] | 293 |
Detector technology | AREA DETECTOR |
Collection date | 1992-10-04 |
Detector | SIEMENS |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 26.345, 55.885, 31.550 |
Unit cell angles | 90.00, 109.98, 90.00 |
Refinement procedure
Resolution | 10.000 - 2.100 |
R-factor | 0.194 * |
Rwork | 0.194 |
R-free | 0.28300 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | THE 38% RELATIVE HUMIDITY FORM I STRUCTURE |
RMSD bond length | 0.012 |
RMSD bond angle | 0.044 |
Data reduction software | XENGEN |
Data scaling software | XENGEN |
Phasing software | X-PLOR |
Refinement software | PROLSQ |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 10.000 | 2.144 |
High resolution limit [Å] | 2.100 | 2.061 |
Rmerge | 0.063 | 0.307 |
Total number of observations | 13358 * | |
Number of reflections | 4847 | |
<I/σ(I)> | 14.08 | 2.55 |
Completeness [%] | 90.5 | 48.5 |
Redundancy | 2.76 | 1.65 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 4.6 | pH 4.6 |