1W2K
tf7a_4380 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 1996-09-16 |
Detector | MARRESEARCH |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 71.874, 82.638, 123.722 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.820 - 3.000 |
Rwork | 0.197 |
R-free | 0.25700 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1w0y |
RMSD bond length | 0.006 |
RMSD bond angle | 1.400 |
Data reduction software | XDS |
Data scaling software | XDS |
Refinement software | CNX (2002) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.870 | 3.200 |
High resolution limit [Å] | 3.000 | 3.000 |
Rmerge | 0.160 | 0.290 |
Number of reflections | 14546 | |
<I/σ(I)> | 12.15 | 5.02 |
Completeness [%] | 95.0 | 92.8 |
Redundancy | 3.45 | 3.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5.5 | pH 5.50 |