1VZD
L. CASEI THYMIDYLATE SYNTHASE MUTANT E60Q TERNARY COMPLEX WITH FDUMP AND CB3717
Experimental procedure
Detector technology | IMAGE PLATE |
Collection date | 1994-04-05 |
Detector | RIGAKU RAXIS IIC |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 78.500, 78.500, 230.600 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 15.000 - 2.500 |
R-factor | 0.188 |
Rwork | 0.188 |
RMSD bond length | 0.022 |
RMSD bond angle | 27.580 |
Data reduction software | PROCESS |
Data scaling software | PROCESS |
Phasing software | X-PLOR (3.1) |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 15.000 * |
High resolution limit [Å] | 2.500 * |
Rmerge | 0.115 |
Number of reflections | 10269 |
Completeness [%] | 60.7 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion * | 6.8 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | potassium phosphate | 20 (mM) | |
2 | 1 | drop | enzyme | 10 (mg/ml) | |
3 | 1 | drop | ammonium sulfate | 15-20 (mM) | |
4 | 1 | drop | dUMP | 5 (mM) | |
5 | 1 | drop | potassium phosphate | 20 (mM) |