Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RU300 |
| Temperature [K] | 298 |
| Detector technology | IMAGE PLATE |
| Collection date | 2002-09-10 |
| Detector | RIGAKU RAXIS IV |
| Wavelength(s) | 1.5418 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 38.420, 51.000, 104.200 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 8.000 - 2.000 |
| R-factor | 0.212 |
| Rwork | 0.171 |
| R-free | 0.20900 |
| Structure solution method | FOURIER SYNTHESIS |
| RMSD bond length | 0.680 |
| RMSD bond angle | 1.700 |
| Data reduction software | bioteX |
| Data scaling software | d*TREK (7.2SSIbeta) |
| Refinement software | CNS |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.620 | 1.800 |
| High resolution limit [Å] | 1.730 | 1.730 |
| Number of reflections | 16006 | |
| Completeness [%] | 71.6 | 10.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 5.6 | 298 | Mg formate, pH 5.6, VAPOR DIFFUSION, HANGING DROP, temperature 298K |
