1UHL
Crystal structure of the LXRalfa-RXRbeta LBD heterodimer
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | MAX II BEAMLINE I711 |
| Synchrotron site | MAX II |
| Beamline | I711 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2002-09-02 |
| Detector | MARRESEARCH |
| Wavelength(s) | 1.11 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 67.634, 88.996, 90.795 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 19.650 - 2.900 |
| R-factor | 0.2239 |
| Rwork | 0.219 |
| R-free | 0.32649 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1dkf |
| RMSD bond length | 0.029 |
| RMSD bond angle | 2.776 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.1.24) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 19.650 | 3.000 |
| High resolution limit [Å] | 2.900 | 2.900 |
| Number of reflections | 12550 | |
| <I/σ(I)> | 9.2 | 1.9 |
| Completeness [%] | 99.9 | 99.8 |
| Redundancy | 6.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 305 | MES, PEG, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 305K |
