1RLD

SOLID-STATE PHASE TRANSITION IN THE CRYSTAL STRUCTURE OF RIBULOSE 1,5-BIPHOSPHATE CARBOXYLASE(SLASH)OXYGENASE

Experimental procedure

Spacegroup name	I 4
Unit cell lengths	153.010, 153.010, 113.450
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	8.000 - 2.500
R-factor	0.211
Rwork	0.211
RMSD bond length	0.018
RMSD bond angle	3.830
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall
High resolution limit [Å]	2.500 *
Rmerge	0.083 *
Number of reflections	38575 *
Completeness [%]	84.0 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *	5.2 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir		0.2 (M)
2	1	reservoir		0.3 (M)
3	1	reservoir		1 (mM)
4	1	drop	precipitant	30-70 (%(v/v))