1POP

X-RAY CRYSTALLOGRAPHIC STRUCTURE OF A PAPAIN-LEUPEPTIN COMPLEX

Experimental procedure

Spacegroup name	P 21 21 21
Unit cell lengths	44.920, 104.960, 50.970
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	20.000 * - 2.100
R-factor	0.198 *
RMSD bond length	0.013
RMSD bond angle	2.330
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall
High resolution limit [Å]	2.100 *
Rmerge	0.094 *
Number of reflections	12452 *
Completeness [%]	88.0 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, sitting drop *		4 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	H2O-methanol		0.5ml
2	1	reservoir			0.060mlsat
3	1	drop	inhibited papain		0.030ml