1PE6

REFINED X-RAY STRUCTURE OF PAPAIN(DOT)E-64-C COMPLEX AT 2.1-ANGSTROMS RESOLUTION

Experimental procedure

Spacegroup name	P 21 21 21
Unit cell lengths	42.900, 95.510, 49.990
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	6.000 - 2.100
R-factor	0.159
RMSD bond length	0.011
RMSD bond angle	0.040
Refinement software	PROLSQ

Data quality characteristics

	Overall
High resolution limit [Å]	2.100 *
Rmerge	0.027 *
Number of reflections	12794 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *		20 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	enzyme	1.5 (%(w/v))
2	1	drop		7.6 (mM)
3	1	drop	methanol	42.6 (%(w/v))
4	1	drop	ethanol	21.3 (%(w/v))