1NHX
PEPCK COMPLEX WITH A GTP-COMPETITIVE INHIBITOR
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU |
| Temperature [K] | 110 |
| Detector technology | IMAGE PLATE |
| Collection date | 1999-05-14 |
| Detector | MARRESEARCH |
| Wavelength(s) | 1.5418 |
| Spacegroup name | P 1 |
| Unit cell lengths | 45.383, 61.452, 62.265 |
| Unit cell angles | 89.71, 70.24, 72.56 |
Refinement procedure
| Resolution | 50.000 - 2.100 |
| R-factor | 0.17532 |
| Rwork | 0.173 |
| R-free | 0.21718 |
| Structure solution method | RIGID-BODY REFINEMENT |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.131 |
| Data scaling software | SCALEPACK |
| Refinement software | REFMAC (5.1.24) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 25.000 | 2.170 |
| High resolution limit [Å] | 2.100 | 2.100 |
| Number of reflections | 32199 | |
| <I/σ(I)> | 23.5 | |
| Completeness [%] | 91.3 | 84 |
| Redundancy | 2.2 | 2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | unknown * |
