1EJH
EIF4E/EIF4G PEPTIDE/7-METHYL-GDP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CHESS BEAMLINE A1 |
Synchrotron site | CHESS |
Beamline | A1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 1998-10-01 |
Detector | ADSC QUANTUM 1 |
Spacegroup name | P 31 |
Unit cell lengths | 140.600, 140.600, 39.400 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 20.000 - 2.200 |
Rwork | 0.218 |
R-free | 0.26100 |
RMSD bond length | 0.007 |
RMSD bond angle | 1.290 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.280 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.093 | 0.206 |
Completeness [%] | 98.9 | 95.8 |
Redundancy | 3 | 3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 277 | (NH4)2SO4 and Peg400, pH 8.5, VAPOR DIFFUSION, HANGING DROP |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | ammonium sulfate | 2.0-2.1 (M) | |
2 | 1 | reservoir | PEG400 | 5 (%) | |
3 | 1 | reservoir | EDTA | 10 (mM) | |
4 | 1 | reservoir | Tris-HCl | 0.1 (M) |