1DVJ

CRYSTAL STRUCTURE OF OROTIDINE MONOPHOSPHATE DECARBOXYLASE COMPLEXED WITH 6-AZAUMP

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS
Synchrotron site	APS
Temperature [K]	100
Detector technology	CCD
Collection date	1999-06-15
Detector	ADSC QUANTUM 4
Spacegroup name	P 1 21 1
Unit cell lengths	72.950, 98.620, 73.250
Unit cell angles	90.00, 104.03, 90.00

Refinement procedure

Resolution	30.000 - 1.500
R-factor	0.174
Rwork	0.174
R-free	0.18800
RMSD bond length	0.015
RMSD bond angle	1.700
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	AMoRE
Refinement software	CNS (0.5)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	30.000	1.580
High resolution limit [Å]	1.500	1.500
Rmerge	0.058	0.326
Total number of observations	1127371 *
Number of reflections	156498
<I/σ(I)>	8.9
Completeness [%]	97.6	87.9
Redundancy	7.2	6.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *	6.5	298	unpublished data *