1CDO
ALCOHOL DEHYDROGENASE (E.C.1.1.1.1) (EE ISOZYME) COMPLEXED WITH NICOTINAMIDE ADENINE DINUCLEOTIDE (NAD), AND ZINC
Experimental procedure
Source type | SYNCHROTRON |
Source details | EMBL/DESY, HAMBURG BEAMLINE X11 |
Synchrotron site | EMBL/DESY, HAMBURG |
Beamline | X11 |
Detector technology | IMAGE PLATE |
Collection date | 1994-05 |
Detector | MARRESEARCH |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 102.950, 47.600, 80.430 |
Unit cell angles | 90.00, 104.66, 90.00 |
Refinement procedure
Resolution | 7.000 - 2.050 |
R-factor | 0.177 |
Rwork | 0.177 |
R-free | 0.24800 |
RMSD bond length | 0.010 |
RMSD bond angle | 25.100 * |
Data reduction software | DENZO |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | Outer shell | |
High resolution limit [Å] | 2.050 * | 2.050 * |
Rmerge | 0.120 | |
Total number of observations | 83875 * | |
Number of reflections | 39749 | |
Completeness [%] | 86.9 | 73.7 * |
Redundancy | 2.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 6.9 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | TES | 50 (mM) | |
2 | 1 | reservoir | NAD | 10 (mM) | |
3 | 1 | reservoir | pyrazole | 1 (mM) | |
4 | 1 | reservoir | PEG2000 | 15.2 (%) |