1BF2
STRUCTURE OF PSEUDOMONAS ISOAMYLASE
Experimental procedure
Source type | ROTATING ANODE |
Source details | RIGAKU RUH2R |
Temperature [K] | 298 |
Detector technology | IMAGE PLATE |
Collection date | 1994-05-24 |
Detector | RIGAKU |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 138.900, 152.400, 53.500 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 10.000 - 2.000 |
R-factor | 0.161 |
Rwork | 0.161 |
R-free | 0.21400 |
RMSD bond length | 0.009 * |
RMSD bond angle | 1.769 * |
Phasing software | X-PLOR (3.1) |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 17.000 |
High resolution limit [Å] | 2.200 |
Rmerge | 0.078 |
Total number of observations | 186961 * |
Number of reflections | 57176 |
Completeness [%] | 97.1 |
Redundancy | 3.27 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Microdialysis * | 4.8 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | protein | 20 (mg/ml) | |
2 | 1 | 2 | ammonium sulfate | 0.6 (M) | pH4.8 |