1ACJ
QUATERNARY LIGAND BINDING TO AROMATIC RESIDUES IN THE ACTIVE-SITE GORGE OF ACETYLCHOLINESTERASE
Experimental procedure
| Spacegroup name | P 31 2 1 |
| Unit cell lengths | 113.700, 113.700, 138.100 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 8.000 - 2.800 |
| R-factor | 0.195 |
| Rwork | 0.195 |
| RMSD bond length | 0.025 |
| Phasing software | X-PLOR |
| Refinement software | X-PLOR |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Microdialysis * | 7.4 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | 1 | protein | 10 (mg/ml) | |
| 2 | 1 | 1 | phosphate | 0.05 (M) | |
| 3 | 1 | 2 | ammonium sulfate | 37-42 (%sat) | |
| 4 | 1 | 2 | phosphate | 0.05 (M) |
