138D
A-DNA DECAMER D(GCGGGCCCGC)-HEXAGONAL CRYSTAL FORM
Experimental procedure
| Source type | ROTATING ANODE |
| Temperature [K] | 290 |
| Detector technology | AREA DETECTOR |
| Detector | SIEMENS |
| Spacegroup name | P 61 2 2 |
| Unit cell lengths | 39.110, 39.110, 79.230 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 8.000 - 1.800 |
| R-factor | 0.183 |
| Rwork | 0.183 |
| RMSD bond length | 0.017 |
| RMSD bond angle | 3.600 |
| Refinement software | X-PLOR |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 15.000 |
| High resolution limit [Å] | 1.800 |
| Rmerge | 0.039 * |
| Total number of observations | 19222 * |
| Number of reflections | 3435 |
| Completeness [%] | 91.0 * |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7 | pH 7.00, VAPOR DIFFUSION, HANGING DROP |
Crystallization Reagents
| ID | crystal ID | solution ID | reagent name | concentration | details |
| 1 | 1 | 1 | WATER | ||
| 2 | 1 | 1 | NA CACODYLATE | ||
| 3 | 1 | 1 | [CO(NH3)6]CL3 | ||
| 4 | 1 | 2 | WATER | ||
| 5 | 1 | 2 | MPD |
