138D

A-DNA DECAMER D(GCGGGCCCGC)-HEXAGONAL CRYSTAL FORM

Experimental procedure

Source type	ROTATING ANODE
Temperature [K]	290
Detector technology	AREA DETECTOR
Detector	SIEMENS
Spacegroup name	P 61 2 2
Unit cell lengths	39.110, 39.110, 79.230
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	8.000 - 1.800
R-factor	0.183
Rwork	0.183
RMSD bond length	0.017
RMSD bond angle	3.600
Refinement software	X-PLOR

Data quality characteristics

	Overall
Low resolution limit [Å]	15.000
High resolution limit [Å]	1.800
Rmerge	0.039 *
Total number of observations	19222 *
Number of reflections	3435
Completeness [%]	91.0 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	7		pH 7.00, VAPOR DIFFUSION, HANGING DROP

Crystallization Reagents

ID	crystal ID	solution ID	reagent name	concentration	details
1	1	1	WATER
2	1	1	NA CACODYLATE
3	1	1	[CO(NH3)6]CL3
4	1	2	WATER
5	1	2	MPD