105M
SPERM WHALE MYOGLOBIN N-BUTYL ISOCYANIDE AT PH 9.0
Experimental procedure
Source type | ROTATING ANODE |
Source details | SIEMENS |
Temperature [K] | 292 |
Detector technology | IMAGE PLATE |
Collection date | 1993-07 |
Detector | RIGAKU |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 64.720, 30.061, 35.191 |
Unit cell angles | 90.00, 105.76, 90.00 |
Refinement procedure
Resolution | 5.000 - 2.020 |
R-factor | 0.174 |
Rwork | 0.174 |
R-free | 0.26800 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | SPERM WHALE MYOGLOBIN NBNC WITHOUT LIGAND |
RMSD bond length | 0.007 |
RMSD bond angle | 1.200 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | X-PLOR (3.851) |
Refinement software | X-PLOR (3.851) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 6.000 | 2.030 |
High resolution limit [Å] | 2.020 | 2.020 |
Rmerge | 0.071 | 0.225 |
Number of reflections | 7987 | |
Completeness [%] | 90.7 | 90.9 |
Redundancy | 1.82 | 1.96 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 9 | 3.0 M AMMONIUM SULFATE, UNBUFFERED, pH 9.0 |