手法: 蒸気拡散法 / pH: 7 詳細: 0.01 M inhibitor, 0.01 M magnesium chloride, 0.01 M ATP were added to the protein sample. Crystal condition: 2.5 M ammonium sulfate, 0.1 M BTP, 1.1 % w/v Cyclohexylethanoyl-N- ...詳細: 0.01 M inhibitor, 0.01 M magnesium chloride, 0.01 M ATP were added to the protein sample. Crystal condition: 2.5 M ammonium sulfate, 0.1 M BTP, 1.1 % w/v Cyclohexylethanoyl-N-hydroxyethylglucamide., pH 7.0, vapor diffusion
解像度: 1.8→26.532 Å / Cor.coef. Fo:Fc: 0.967 / Cor.coef. Fo:Fc free: 0.951 / WRfactor Rfree: 0.208 / WRfactor Rwork: 0.167 / Occupancy max: 1 / Occupancy min: 0.3 / SU B: 6.661 / SU ML: 0.099 / 交差検証法: THROUGHOUT / σ(F): 0 / ESU R: 0.126 / ESU R Free: 0.124 / 立体化学のターゲット値: MAXIMUM LIKELIHOOD 詳細: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS U VALUES: WITH TLS ADDED. INHIBITOR RESTRAINTS WERE BASED ON PRODRG CALCULATIONS. COOT AND THE MOLPROBITY SERVER WERE ALSO USED DURING ...詳細: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS U VALUES: WITH TLS ADDED. INHIBITOR RESTRAINTS WERE BASED ON PRODRG CALCULATIONS. COOT AND THE MOLPROBITY SERVER WERE ALSO USED DURING REFINEMENT. SOME DUMMY ATOMS AND PHOSPHATE IONS B303, B304, A303, B305 OF THE MODEL REPRESENT ELECTRON DENSITY THAT APPEARS TO ARISE FROM A LARGER, UNIDENTIFIED MOLECULE.
Rfactor
反射数
%反射
Selection details
Rfree
0.2198
2074
4.25 %
thin shells (sftools)
Rwork
0.1761
-
-
-
obs
0.178
48796
99.227 %
-
溶媒の処理
イオンプローブ半径: 0.8 Å / 減衰半径: 0.8 Å / VDWプローブ半径: 1.2 Å / 溶媒モデル: MASK BULK SOLVENT