PDB-3u8k: Crystal structure of the acetylcholine binding protein (AChBP) fr...

基本情報

• 登録情報: データベース: PDB / ID: 3u8k
• タイトル: Crystal structure of the acetylcholine binding protein (AChBP) from Lymnaea stagnalis in complex with NS3573 (1-(5-ethoxypyridin-3-yl)-1,4-diazepane)
• 要素: Acetylcholine-binding protein
• キーワード: Acetylcholine-binding protein/agonist / Lymnaea stagnalis / agonist / Ligand-bindig domain / Acetylcholine / Acetylcholine-binding protein / Acetylcholine-binding protein-agonist complex

機能・相同性

分子機能:

acetylcholine receptor activity / acetylcholine-gated monoatomic cation-selective channel activity / synaptic cleft / response to nicotine / neuron projection / synapse / membrane

ドメイン・相同性:

Acetylcholine Binding Protein; Chain: A, / Neurotransmitter-gated ion-channel ligand-binding domain / Neurotransmitter-gated ion-channel / Neurotransmitter-gated ion-channel ligand-binding domain / Neurotransmitter-gated ion-channel ligand-binding domain superfamily / Neurotransmitter-gated ion-channel ligand binding domain / Distorted Sandwich / Ig-like domain profile. / Immunoglobulin-like domain / Mainly Beta

構成要素:

1-(5-ethoxypyridin-3-yl)-1,4-diazepane / Acetylcholine-binding protein

• 生物種: Lymnaea stagnalis (無脊椎動物)
• 手法: X線回折 / シンクロトロン / 分子置換 / 解像度: 2.47 Å
• データ登録者: Rohde, L.A.H. / Ahring, P.K. / Jensen, M.L. / Nielsen, E.O. / Peters, D. / Helgstrand, C. / Krintel, C. / Harpsoe, K. / Gajhede, M. / Kastrup, J.S. / Balle, T.
• 引用: ジャーナル: J.Biol.Chem. / 年: 2012; タイトル: Intersubunit bridge formation governs agonist efficacy at nicotinic acetylcholine alpha 4 beta 2 receptors: unique role of halogen bonding revealed.; 著者: Rohde, L.A. / Ahring, P.K. / Jensen, M.L. / Nielsen, E. / Peters, D. / Helgstrand, C. / Krintel, C. / Harpse, K. / Gajhede, M. / Kastrup, J.S. / Balle, T.

履歴

登録	2011年10月17日	登録サイト: RCSB / 処理サイト: RCSB
改定 1.0	2011年12月14日	Provider: repository / タイプ: Initial release
改定 1.1	2013年9月18日	Group: Database references
改定 1.2	2018年3月7日	Group: Data collection / カテゴリ: diffrn_source / Item: _diffrn_source.pdbx_synchrotron_site
改定 1.3	2020年7月29日	Group: Data collection / Derived calculations / Structure summary カテゴリ: chem_comp / entity / pdbx_chem_comp_identifier / pdbx_entity_nonpoly / struct_conn / struct_site / struct_site_gen Item: _chem_comp.name / _chem_comp.type / _entity.pdbx_description / _pdbx_entity_nonpoly.name / _struct_conn.pdbx_leaving_atom_flag / _struct_conn.pdbx_role / _struct_conn.ptnr1_auth_asym_id / _struct_conn.ptnr1_label_asym_id / _struct_conn.ptnr2_auth_asym_id / _struct_conn.ptnr2_auth_seq_id / _struct_conn.ptnr2_label_asym_id 解説: Carbohydrate remediation / Provider: repository / タイプ: Remediation
改定 1.4	2023年9月13日	Group: Data collection / Database references / Refinement description / Structure summary カテゴリ: chem_comp / chem_comp_atom / chem_comp_bond / database_2 / pdbx_initial_refinement_model Item: _chem_comp.pdbx_synonyms / _database_2.pdbx_DOI / _database_2.pdbx_database_accession

集合体

登録構造単位

A: Acetylcholine-binding protein

B: Acetylcholine-binding protein

C: Acetylcholine-binding protein

D: Acetylcholine-binding protein

E: Acetylcholine-binding protein

F: Acetylcholine-binding protein

G: Acetylcholine-binding protein

H: Acetylcholine-binding protein

I: Acetylcholine-binding protein

J: Acetylcholine-binding protein

K: Acetylcholine-binding protein

L: Acetylcholine-binding protein

M: Acetylcholine-binding protein

N: Acetylcholine-binding protein

O: Acetylcholine-binding protein

P: Acetylcholine-binding protein

Q: Acetylcholine-binding protein

R: Acetylcholine-binding protein

S: Acetylcholine-binding protein

T: Acetylcholine-binding protein

ヘテロ分子

概要:

• 483 kDa, 20 ポリマー

構成要素の詳細:

	分子量 (理論値)	分子数
合計 (水以外)	483,301	53
ポリマ－	477,250	20
非ポリマー	6,050	33
水	24,879	1381

1

A: Acetylcholine-binding protein

B: Acetylcholine-binding protein

C: Acetylcholine-binding protein

D: Acetylcholine-binding protein

E: Acetylcholine-binding protein

ヘテロ分子

概要:

• 登録者・ソフトウェアが定義した集合体
• 121 kDa, 5 ポリマー

構成要素の詳細:

	分子量 (理論値)	分子数
合計 (水以外)	120,832	13
ポリマ－	119,313	5
非ポリマー	1,520	8
水	90	5

対称操作:

タイプ	名称	対称操作	数
identity operation	1_555	x,y,z	1

計算値:

Buried area	14490 Å2
ΔGint	-75 kcal/mol
Surface area	42910 Å2
手法	PISA

2

F: Acetylcholine-binding protein

G: Acetylcholine-binding protein

H: Acetylcholine-binding protein

I: Acetylcholine-binding protein

J: Acetylcholine-binding protein

ヘテロ分子

概要:

• 登録者・ソフトウェアが定義した集合体
• 121 kDa, 5 ポリマー

構成要素の詳細:

	分子量 (理論値)	分子数
合計 (水以外)	120,832	13
ポリマ－	119,313	5
非ポリマー	1,520	8
水	90	5

対称操作:

タイプ	名称	対称操作	数
identity operation	1_555	x,y,z	1

計算値:

Buried area	14050 Å2
ΔGint	-62 kcal/mol
Surface area	43070 Å2
手法	PISA

3

K: Acetylcholine-binding protein

L: Acetylcholine-binding protein

M: Acetylcholine-binding protein

N: Acetylcholine-binding protein

O: Acetylcholine-binding protein

ヘテロ分子

概要:

• 登録者・ソフトウェアが定義した集合体
• 121 kDa, 5 ポリマー

構成要素の詳細:

	分子量 (理論値)	分子数
合計 (水以外)	120,803	14
ポリマ－	119,313	5
非ポリマー	1,491	9
水	90	5

対称操作:

タイプ	名称	対称操作	数
identity operation	1_555	x,y,z	1

計算値:

Buried area	14590 Å2
ΔGint	-113 kcal/mol
Surface area	42780 Å2
手法	PISA

4

P: Acetylcholine-binding protein

Q: Acetylcholine-binding protein

R: Acetylcholine-binding protein

S: Acetylcholine-binding protein

T: Acetylcholine-binding protein

ヘテロ分子

概要:

• 登録者・ソフトウェアが定義した集合体
• 121 kDa, 5 ポリマー

構成要素の詳細:

	分子量 (理論値)	分子数
合計 (水以外)	120,832	13
ポリマ－	119,313	5
非ポリマー	1,520	8
水	90	5

対称操作:

タイプ	名称	対称操作	数
identity operation	1_555	x,y,z	1

計算値:

Buried area	14200 Å2
ΔGint	-73 kcal/mol
Surface area	41640 Å2
手法	PISA

単位格子

Length a, b, c (Å)	235.410, 273.160, 73.580
Angle α, β, γ (deg.)	90.00, 90.00, 90.00
Int Tables number	18
Space group name H-M	P21212

非結晶学的対称性 (NCS)

NCSドメイン:

ID	Ens-ID
1	1
2	1
3	1
4	1
5	1
6	1
7	1
8	1
9	1
10	1
11	1
12	1
13	1
14	1
15	1
16	1
17	1
18	1
19	1
20	1
1	2
2	2
3	2
4	2
5	2
6	2
7	2
8	2
9	2
10	2
11	2
12	2
13	2
14	2
15	2
16	2
17	2
18	2
19	2
20	2
1	3
2	3
3	3
4	3
5	3
6	3
7	3
8	3
9	3
10	3
11	3
12	3
13	3
14	3
15	3
16	3
17	3
18	3
19	3
20	3
1	4
2	4
3	4
4	4
5	4
6	4
7	4
8	4
9	4
10	4
11	4
12	4
13	4
14	4
15	4
16	4
17	4
18	4
1	5
2	5
1	6
2	6
3	6
4	6
5	6
6	6
7	6
8	6
9	6
10	6
11	6
12	6
13	6
14	6
15	6
16	6
17	6
18	6
19	6
20	6
1	7
2	7
3	7
4	7
5	7
6	7
7	7
8	7
9	7
10	7
11	7
12	7
13	7
14	7
15	7
16	7
17	7
18	7
19	7
20	7
1	8
2	8
3	8
4	8
5	8
6	8
7	8
8	8
9	8
10	8
11	8
12	8
13	8
14	8
15	8
16	8
17	8
18	8
19	8
20	8
1	9
2	9
3	9
4	9
5	9
6	9
7	9
8	9
9	9
10	9
11	9
12	9
13	9
14	9
15	9
16	9
17	9
1	10
2	10
3	10
1	11
2	11
3	11
4	11
5	11
6	11
7	11
8	11
9	11
10	11
11	11
12	11
13	11
14	11
15	11
16	11
17	11
18	11
19	11
20	11
1	12
2	12
3	12
1	13
2	13
3	13
4	13
5	13
6	13
7	13
8	13
9	13
10	13
11	13
12	13
13	13
14	13
15	13
16	13
17	13
1	14
2	14
3	14
4	14
5	14
6	14
7	14
8	14
9	14
10	14
11	14
12	14
13	14
14	14
15	14
16	14
17	14
18	14
19	14
20	14
1	15
2	15
3	15
4	15
5	15
6	15
7	15
8	15
9	15
10	15
11	15
12	15
13	15
14	15
15	15
16	15
17	15
1	16
2	16
3	16
1	17
2	17
3	17
4	17
5	17
1	18
2	18
3	18
4	18
5	18
6	18
7	18
8	18
9	18
10	18
1	19
2	19
3	19
4	19
1	20
2	20
3	20
4	20
5	20
6	20
7	20
8	20
9	20
10	20
11	20
12	20
13	20
14	20
15	20
16	20
17	20
18	20
19	20
20	20

NCSドメイン領域:

Dom-ID	Component-ID	Ens-ID	Selection details
1	1	1	chain A and resid 1:12
2	1	1	chain B and resid 1:12
3	1	1	chain C and resid 1:12
4	1	1	chain D and resid 1:12
5	1	1	chain E and resid 1:12
6	1	1	chain F and resid 1:12
7	1	1	chain G and resid 1:12
8	1	1	chain H and resid 1:12
9	1	1	chain I and resid 1:12
10	1	1	chain J and resid 1:12
11	1	1	chain K and resid 1:12
12	1	1	chain L and resid 1:12
13	1	1	chain M and resid 1:12
14	1	1	chain N and resid 1:12
15	1	1	chain O and resid 1:12
16	1	1	chain P and resid 1:12
17	1	1	chain Q and resid 1:12
18	1	1	chain R and resid 1:12
19	1	1	chain S and resid 1:12
20	1	1	chain T and resid 1:12
1	1	2	chain A and resid 16:22
2	1	2	chain B and resid 16:22
3	1	2	chain C and resid 16:22
4	1	2	chain D and resid 16:22
5	1	2	chain E and resid 16:22
6	1	2	chain F and resid 16:22
7	1	2	chain G and resid 16:22
8	1	2	chain H and resid 16:22
9	1	2	chain I and resid 16:22
10	1	2	chain J and resid 16:22
11	1	2	chain K and resid 16:22
12	1	2	chain L and resid 16:22
13	1	2	chain M and resid 16:22
14	1	2	chain N and resid 16:22
15	1	2	chain O and resid 16:22
16	1	2	chain P and resid 16:22
17	1	2	chain Q and resid 16:22
18	1	2	chain R and resid 16:22
19	1	2	chain S and resid 16:22
20	1	2	chain T and resid 16:22
1	1	3	chain A and resid 26:60
2	1	3	chain B and resid 26:60
3	1	3	chain C and resid 26:60
4	1	3	chain D and resid 26:60
5	1	3	chain E and resid 26:60
6	1	3	chain F and resid 26:60
7	1	3	chain G and resid 26:60
8	1	3	chain H and resid 26:60
9	1	3	chain I and resid 26:60
10	1	3	chain J and resid 26:60
11	1	3	chain K and resid 26:60
12	1	3	chain L and resid 26:60
13	1	3	chain M and resid 26:60
14	1	3	chain N and resid 26:60
15	1	3	chain O and resid 26:60
16	1	3	chain P and resid 26:60
17	1	3	chain Q and resid 26:60
18	1	3	chain R and resid 26:60
19	1	3	chain S and resid 26:60
20	1	3	chain T and resid 26:60
1	1	4	chain A and resid 61
2	1	4	chain B and resid 61
3	1	4	chain C and resid 61
4	1	4	chain D and resid 61
5	1	4	chain E and resid 61
6	1	4	chain F and resid 61
7	1	4	chain G and resid 61
8	1	4	chain H and resid 61
9	1	4	chain I and resid 61
10	1	4	chain J and resid 61
11	1	4	chain K and resid 61
12	1	4	chain L and resid 61
13	1	4	chain M and resid 61
14	1	4	chain N and resid 61
15	1	4	chain O and resid 61
16	1	4	chain Q and resid 61
17	1	4	chain S and resid 61
18	1	4	chain T and resid 61
1	1	5	chain P and resid 61
2	1	5	chain R and resid 61
1	1	6	chain A and resid 62:67
2	1	6	chain B and resid 62:67
3	1	6	chain C and resid 62:67
4	1	6	chain D and resid 62:67
5	1	6	chain E and resid 62:67
6	1	6	chain F and resid 62:67
7	1	6	chain G and resid 62:67
8	1	6	chain H and resid 62:67
9	1	6	chain I and resid 62:67
10	1	6	chain J and resid 62:67
11	1	6	chain K and resid 62:67
12	1	6	chain L and resid 62:67
13	1	6	chain M and resid 62:67
14	1	6	chain N and resid 62:67
15	1	6	chain O and resid 62:67
16	1	6	chain P and resid 62:67
17	1	6	chain Q and resid 62:67
18	1	6	chain R and resid 62:67
19	1	6	chain S and resid 62:67
20	1	6	chain T and resid 62:67
1	1	7	chain A and resid 68:69
2	1	7	chain B and resid 68:69
3	1	7	chain C and resid 68:69
4	1	7	chain D and resid 68:69
5	1	7	chain E and resid 68:69
6	1	7	chain F and resid 68:69
7	1	7	chain G and resid 68:69
8	1	7	chain H and resid 68:69
9	1	7	chain I and resid 68:69
10	1	7	chain J and resid 68:69
11	1	7	chain K and resid 68:69
12	1	7	chain L and resid 68:69
13	1	7	chain M and resid 68:69
14	1	7	chain N and resid 68:69
15	1	7	chain O and resid 68:69
16	1	7	chain P and resid 68:69
17	1	7	chain Q and resid 68:69
18	1	7	chain R and resid 68:69
19	1	7	chain S and resid 68:69
20	1	7	chain T and resid 68:69
1	1	8	chain A and resid 70:128
2	1	8	chain B and resid 70:128
3	1	8	chain C and resid 70:128
4	1	8	chain D and resid 70:128
5	1	8	chain E and resid 70:128
6	1	8	chain F and resid 70:128
7	1	8	chain G and resid 70:128
8	1	8	chain H and resid 70:128
9	1	8	chain I and resid 70:128
10	1	8	chain J and resid 70:128
11	1	8	chain K and resid 70:128
12	1	8	chain L and resid 70:128
13	1	8	chain M and resid 70:128
14	1	8	chain N and resid 70:128
15	1	8	chain O and resid 70:128
16	1	8	chain P and resid 70:128
17	1	8	chain Q and resid 70:128
18	1	8	chain R and resid 70:128
19	1	8	chain S and resid 70:128
20	1	8	chain T and resid 70:128
1	1	9	chain A and resid 129:131
2	1	9	chain B and resid 129:131
3	1	9	chain C and resid 129:131
4	1	9	chain D and resid 129:131
5	1	9	chain E and resid 129:131
6	1	9	chain F and resid 129:131
7	1	9	chain G and resid 129:131
8	1	9	chain H and resid 129:131
9	1	9	chain J and resid 129:131
10	1	9	chain K and resid 129:131
11	1	9	chain M and resid 129:131
12	1	9	chain N and resid 129:131
13	1	9	chain O and resid 129:131
14	1	9	chain Q and resid 129:131
15	1	9	chain R and resid 129:131
16	1	9	chain S and resid 129:131
17	1	9	chain T and resid 129:131
1	1	10	chain I and resid 129:131
2	1	10	chain P and resid 129:131
3	1	10	chain L and resid 129:131
1	1	11	chain A and resid 132:147
2	1	11	chain B and resid 132:147
3	1	11	chain C and resid 132:147
4	1	11	chain D and resid 132:147
5	1	11	chain E and resid 132:147
6	1	11	chain F and resid 132:147
7	1	11	chain G and resid 132:147
8	1	11	chain H and resid 132:147
9	1	11	chain I and resid 132:147
10	1	11	chain J and resid 132:147
11	1	11	chain K and resid 132:147
12	1	11	chain L and resid 132:147
13	1	11	chain M and resid 132:147
14	1	11	chain N and resid 132:147
15	1	11	chain O and resid 132:147
16	1	11	chain P and resid 132:147
17	1	11	chain Q and resid 132:147
18	1	11	chain R and resid 132:147
19	1	11	chain S and resid 132:147
20	1	11	chain T and resid 132:147
1	1	12	chain A and resid 148:155
2	1	12	chain I and resid 148:155
3	1	12	chain R and resid 148:155
1	1	13	chain B and resid 148:155
2	1	13	chain C and resid 148:155
3	1	13	chain D and resid 148:155
4	1	13	chain E and resid 148:155
5	1	13	chain F and resid 148:155
6	1	13	chain G and resid 148:155
7	1	13	chain H and resid 148:155
8	1	13	chain J and resid 148:155
9	1	13	chain K and resid 148:155
10	1	13	chain L and resid 148:155
11	1	13	chain M and resid 148:155
12	1	13	chain N and resid 148:155
13	1	13	chain O and resid 148:155
14	1	13	chain P and resid 148:155
15	1	13	chain Q and resid 148:155
16	1	13	chain S and resid 148:155
17	1	13	chain T and resid 148:155
1	1	14	chain A and resid 163:183
2	1	14	chain B and resid 163:183
3	1	14	chain C and resid 163:183
4	1	14	chain D and resid 163:183
5	1	14	chain E and resid 163:183
6	1	14	chain F and resid 163:183
7	1	14	chain G and resid 163:183
8	1	14	chain H and resid 163:183
9	1	14	chain I and resid 163:183
10	1	14	chain J and resid 163:183
11	1	14	chain K and resid 163:183
12	1	14	chain L and resid 163:183
13	1	14	chain M and resid 163:183
14	1	14	chain N and resid 163:183
15	1	14	chain O and resid 163:183
16	1	14	chain P and resid 163:183
17	1	14	chain Q and resid 163:183
18	1	14	chain R and resid 163:183
19	1	14	chain S and resid 163:183
20	1	14	chain T and resid 163:183
1	1	15	chain A and resid 184:186
2	1	15	chain C and resid 184:186
3	1	15	chain D and resid 184:186
4	1	15	chain E and resid 184:186
5	1	15	chain F and resid 184:186
6	1	15	chain G and resid 184:186
7	1	15	chain H and resid 184:186
8	1	15	chain I and resid 184:186
9	1	15	chain J and resid 184:186
10	1	15	chain K and resid 184:186
11	1	15	chain L and resid 184:186
12	1	15	chain N and resid 184:186
13	1	15	chain O and resid 184:186
14	1	15	chain Q and resid 184:186
15	1	15	chain R and resid 184:186
16	1	15	chain S and resid 184:186
17	1	15	chain T and resid 184:186
1	1	16	chain B and resid 184:186
2	1	16	chain M and resid 184:186
3	1	16	chain P and resid 184:186
1	1	17	chain B and resid 187:188
2	1	17	chain F and resid 187:188
3	1	17	chain G and resid 187:188
4	1	17	chain H and resid 187:188
5	1	17	chain O and resid 187:188
1	1	18	chain D and resid 187:188
2	1	18	chain E and resid 187:188
3	1	18	chain J and resid 187:188
4	1	18	chain K and resid 187:188
5	1	18	chain M and resid 187:188
6	1	18	chain N and resid 187:188
7	1	18	chain P and resid 187:188
8	1	18	chain Q and resid 187:188
9	1	18	chain R and resid 187:188
10	1	18	chain T and resid 187:188
1	1	19	chain C and resid 187:188
2	1	19	chain I and resid 187:188
3	1	19	chain L and resid 187:188
4	1	19	chain S and resid 187:188
1	1	20	chain A and resid 189:204
2	1	20	chain B and resid 189:204
3	1	20	chain C and resid 189:204
4	1	20	chain D and resid 189:204
5	1	20	chain E and resid 189:204
6	1	20	chain F and resid 189:204
7	1	20	chain G and resid 189:204
8	1	20	chain H and resid 189:204
9	1	20	chain I and resid 189:204
10	1	20	chain J and resid 189:204
11	1	20	chain K and resid 189:204
12	1	20	chain L and resid 189:204
13	1	20	chain M and resid 189:204
14	1	20	chain N and resid 189:204
15	1	20	chain O and resid 189:204
16	1	20	chain P and resid 189:204
17	1	20	chain Q and resid 189:204
18	1	20	chain R and resid 189:204
19	1	20	chain S and resid 189:204
20	1	20	chain T and resid 189:204

NCSアンサンブル:

ID
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20

要素

#1: タンパク質

A B C D E F G H I J K L M N O P Q R S T
Acetylcholine-binding protein / ACh-binding protein / AchBP

詳細:

分子量: 23862.523 Da / 分子数: 20 / 由来タイプ: 組換発現 / 由来: (組換発現) Lymnaea stagnalis (無脊椎動物)
発現宿主: Spodoptera frugiperda (ツマジロクサヨトウ)
株 (発現宿主): Sf9 / 参照: UniProt: P58154

#2: 化合物

A-211 B-211 C-211 D-211 E-211 F-211 G-211 H-211 I-211 J-211 K-211 L-211 M-211 N-211 O-211 P-211 Q-211 R-211 S-211 T-211
ChemComp-09P / 1-(5-ethoxypyridin-3-yl)-1,4-diazepane

詳細:

分子量: 221.299 Da / 分子数: 20 / 由来タイプ: 合成 / 式: C₁₂H₁₉N₃O

#3: 糖

A-212 G-213 R-214 ChemComp-NAG / 2-acetamido-2-deoxy-beta-D-glucopyranose / N-acetyl-beta-D-glucosamine / 2-acetamido-2-deoxy-beta-D-glucose / 2-acetamido-2-deoxy-D-glucose / 2-acetamido-2-deoxy-glucose / N-ACETYL-D-GLUCOSAMINE / N-アセチル-β-D-グルコサミン

詳細:

タイプ: D-saccharide, beta linking / 分子量: 221.208 Da / 分子数: 3 / 由来タイプ: 組換発現 / 式: C₈H₁₅NO₆

識別子:

識別子	タイプ	プログラム
DGlcpNAcb	CONDENSED IUPAC CARBOHYDRATE SYMBOL	GMML 1.0
N-acetyl-b-D-glucopyranosamine	COMMON NAME	GMML 1.0
b-D-GlcpNAc	IUPAC CARBOHYDRATE SYMBOL	PDB-CARE 1.0
GlcNAc	SNFG CARBOHYDRATE SYMBOL	GMML 1.0

#4: 化合物

C-212 D-212 H-212 I-212 K-212 M-212 N-212 O-212 P-212 T-212
ChemComp-SO4 / SULFATE ION / 硫酸ジアニオン

詳細:

分子量: 96.063 Da / 分子数: 10 / 由来タイプ: 合成 / 式: SO₄

#5: 水

ChemComp-HOH / water

詳細:

分子量: 18.015 Da / 分子数: 1381 / 由来タイプ: 天然 / 式: H₂O

実験情報

実験

• 実験: 手法: X線回折 / 使用した結晶の数: 1

試料調製

• 結晶: マシュー密度: 2.48 ų/Da / 溶媒含有率: 50.37 %
• 結晶化: 温度: 293 K / pH: 8 ; 詳細: 50mM Tris, 2.0M Ammonium sulfate, 2% PEG 400, pH 8.0, VAPOR DIFFUSION, HANGING DROP, temperature 293K

データ収集

• 回折: 平均測定温度: 100 K
• 放射光源: 由来: シンクロトロン / サイト: MAX II / ビームライン: I911-2 / 波長: 1
• 検出器: タイプ: MAR CCD 165 mm / 検出器: CCD / 日付: 2009年10月29日
• 放射: プロトコル: SINGLE WAVELENGTH / 単色(M)・ラウエ(L): M / 散乱光タイプ: x-ray
• 放射波長: 波長: 1 Å / 相対比: 1
• 反射: 解像度: 2.47→51.514 Å / Num. obs: 168353 / % possible obs: 99.1 % / 冗長度: 3.2 % / B_iso Wilson estimate: 28.3 Ų / R_merge(I) obs: 0.097 / R_sym value: 0.097 / Net I/σ(I): 6.4
• 反射 シェル: 解像度: 2.47→2.61 Å / 冗長度: 3.1 % / R_merge(I) obs: 0.355 / Mean I/σ(I) obs: 2 / R_sym value: 0.355 / % possible all: 98.1

解析

ソフトウェア

名称	バージョン	分類
PHASER		位相決定
PHENIX	(phenix.refine)	精密化
MOSFLM		データ削減
SCALA		データスケーリング

精密化

構造決定の手法: 分子置換
開始モデル: PDB ENTRY 1UW6: PENTAMER, CHAIN A-E

1uw6

解像度: 2.47→51.51 Å / SU ML: 0.33 / Isotropic thermal model: Restrained / σ(F): 1.34 / 位相誤差: 21.88 / 立体化学のターゲット値: ML

	Rfactor	反射数	%反射
Rfree	0.236	8426	5.01 %
Rwork	0.196	-	-
obs	0.2	168237	98.9 %
all	-	169397	-

• 溶媒の処理: 減衰半径: 0.9 Å / VDWプローブ半径: 1.11 Å / 溶媒モデル: FLAT BULK SOLVENT MODEL / B_sol: 45.01 Ų / k_sol: 0.38 e/ų

原子変位パラメータ

B_iso mean: 30.7 Ų

	Baniso -1	Baniso -2	Baniso -3
1-	-7.8517 Å2	0 Å2	0 Å2
2-	-	6.4523 Å2	0 Å2
3-	-	-	1.3994 Å2

精密化ステップ

サイクル: LAST / 解像度: 2.47→51.51 Å

	タンパク質	核酸	リガンド	溶媒	全体
原子数	32318	0	412	1381	34111

拘束条件

Refine-ID	タイプ	Dev ideal	数
X-RAY DIFFRACTION	f_bond_d	0.008	33582
X-RAY DIFFRACTION	f_angle_d	1.011	45732
X-RAY DIFFRACTION	f_dihedral_angle_d	16.408	12277
X-RAY DIFFRACTION	f_chiral_restr	0.064	5183
X-RAY DIFFRACTION	f_plane_restr	0.004	5874

Refine LS restraints NCS

Ens-ID	Dom-ID	Auth asym-ID	数	Refine-ID	タイプ	Rms dev position (Å)
1	1	A	104	X-RAY DIFFRACTION	POSITIONAL
1	2	B	104	X-RAY DIFFRACTION	POSITIONAL	0.035
1	3	C	104	X-RAY DIFFRACTION	POSITIONAL	0.035
1	4	D	104	X-RAY DIFFRACTION	POSITIONAL	0.033
1	5	E	104	X-RAY DIFFRACTION	POSITIONAL	0.033
1	6	F	104	X-RAY DIFFRACTION	POSITIONAL	0.033
1	7	G	104	X-RAY DIFFRACTION	POSITIONAL	0.033
1	8	H	104	X-RAY DIFFRACTION	POSITIONAL	0.03
1	9	I	104	X-RAY DIFFRACTION	POSITIONAL	0.028
1	10	J	104	X-RAY DIFFRACTION	POSITIONAL	0.035
1	11	K	104	X-RAY DIFFRACTION	POSITIONAL	0.035
1	12	L	104	X-RAY DIFFRACTION	POSITIONAL	0.034
1	13	M	104	X-RAY DIFFRACTION	POSITIONAL	0.035
1	14	N	104	X-RAY DIFFRACTION	POSITIONAL	0.031
1	15	O	104	X-RAY DIFFRACTION	POSITIONAL	0.033
1	16	P	104	X-RAY DIFFRACTION	POSITIONAL	0.038
1	17	Q	104	X-RAY DIFFRACTION	POSITIONAL	0.031
1	18	R	104	X-RAY DIFFRACTION	POSITIONAL	0.036
1	19	S	104	X-RAY DIFFRACTION	POSITIONAL	0.035
1	20	T	104	X-RAY DIFFRACTION	POSITIONAL	0.035
2	1	A	53	X-RAY DIFFRACTION	POSITIONAL
2	2	B	53	X-RAY DIFFRACTION	POSITIONAL	0.04
2	3	C	53	X-RAY DIFFRACTION	POSITIONAL	0.033
2	4	D	53	X-RAY DIFFRACTION	POSITIONAL	0.03
2	5	E	53	X-RAY DIFFRACTION	POSITIONAL	0.047
2	6	F	53	X-RAY DIFFRACTION	POSITIONAL	0.036
2	7	G	53	X-RAY DIFFRACTION	POSITIONAL	0.032
2	8	H	53	X-RAY DIFFRACTION	POSITIONAL	0.033
2	9	I	53	X-RAY DIFFRACTION	POSITIONAL	0.033
2	10	J	53	X-RAY DIFFRACTION	POSITIONAL	0.035
2	11	K	53	X-RAY DIFFRACTION	POSITIONAL	0.035
2	12	L	53	X-RAY DIFFRACTION	POSITIONAL	0.032
2	13	M	53	X-RAY DIFFRACTION	POSITIONAL	0.031
2	14	N	53	X-RAY DIFFRACTION	POSITIONAL	0.038
2	15	O	53	X-RAY DIFFRACTION	POSITIONAL	0.04
2	16	P	53	X-RAY DIFFRACTION	POSITIONAL	0.041
2	17	Q	53	X-RAY DIFFRACTION	POSITIONAL	0.037
2	18	R	53	X-RAY DIFFRACTION	POSITIONAL	0.033
2	19	S	44	X-RAY DIFFRACTION	POSITIONAL	0.031
2	20	T	53	X-RAY DIFFRACTION	POSITIONAL	0.032
3	1	A	284	X-RAY DIFFRACTION	POSITIONAL
3	2	B	284	X-RAY DIFFRACTION	POSITIONAL	0.039
3	3	C	284	X-RAY DIFFRACTION	POSITIONAL	0.04
3	4	D	284	X-RAY DIFFRACTION	POSITIONAL	0.042
3	5	E	284	X-RAY DIFFRACTION	POSITIONAL	0.043
3	6	F	284	X-RAY DIFFRACTION	POSITIONAL	0.044
3	7	G	284	X-RAY DIFFRACTION	POSITIONAL	0.042
3	8	H	284	X-RAY DIFFRACTION	POSITIONAL	0.035
3	9	I	284	X-RAY DIFFRACTION	POSITIONAL	0.04
3	10	J	284	X-RAY DIFFRACTION	POSITIONAL	0.044
3	11	K	284	X-RAY DIFFRACTION	POSITIONAL	0.041
3	12	L	284	X-RAY DIFFRACTION	POSITIONAL	0.045
3	13	M	284	X-RAY DIFFRACTION	POSITIONAL	0.038
3	14	N	284	X-RAY DIFFRACTION	POSITIONAL	0.042
3	15	O	284	X-RAY DIFFRACTION	POSITIONAL	0.042
3	16	P	284	X-RAY DIFFRACTION	POSITIONAL	0.04
3	17	Q	284	X-RAY DIFFRACTION	POSITIONAL	0.043
3	18	R	284	X-RAY DIFFRACTION	POSITIONAL	0.042
3	19	S	284	X-RAY DIFFRACTION	POSITIONAL	0.04
3	20	T	284	X-RAY DIFFRACTION	POSITIONAL	0.043
4	1	A	11	X-RAY DIFFRACTION	POSITIONAL
4	2	B	11	X-RAY DIFFRACTION	POSITIONAL	0.013
4	3	C	11	X-RAY DIFFRACTION	POSITIONAL	0.014
4	4	D	11	X-RAY DIFFRACTION	POSITIONAL	0.016
4	5	E	11	X-RAY DIFFRACTION	POSITIONAL	0.022
4	6	F	11	X-RAY DIFFRACTION	POSITIONAL	0.032
4	7	G	11	X-RAY DIFFRACTION	POSITIONAL	0.015
4	8	H	11	X-RAY DIFFRACTION	POSITIONAL	0.016
4	9	I	11	X-RAY DIFFRACTION	POSITIONAL	0.022
4	10	J	11	X-RAY DIFFRACTION	POSITIONAL	0.033
4	11	K	11	X-RAY DIFFRACTION	POSITIONAL	0.024
4	12	L	11	X-RAY DIFFRACTION	POSITIONAL	0.018
4	13	M	11	X-RAY DIFFRACTION	POSITIONAL	0.02
4	14	N	11	X-RAY DIFFRACTION	POSITIONAL	0.024
4	15	O	11	X-RAY DIFFRACTION	POSITIONAL	0.028
4	16	Q	11	X-RAY DIFFRACTION	POSITIONAL	0.028
4	17	S	11	X-RAY DIFFRACTION	POSITIONAL	0.027
4	18	T	11	X-RAY DIFFRACTION	POSITIONAL	0.019
5	1	P	11	X-RAY DIFFRACTION	POSITIONAL
5	2	R	11	X-RAY DIFFRACTION	POSITIONAL	0.043
6	1	A	48	X-RAY DIFFRACTION	POSITIONAL
6	2	B	48	X-RAY DIFFRACTION	POSITIONAL	0.032
6	3	C	48	X-RAY DIFFRACTION	POSITIONAL	0.033
6	4	D	48	X-RAY DIFFRACTION	POSITIONAL	0.03
6	5	E	48	X-RAY DIFFRACTION	POSITIONAL	0.036
6	6	F	48	X-RAY DIFFRACTION	POSITIONAL	0.033
6	7	G	48	X-RAY DIFFRACTION	POSITIONAL	0.048
6	8	H	48	X-RAY DIFFRACTION	POSITIONAL	0.033
6	9	I	48	X-RAY DIFFRACTION	POSITIONAL	0.036
6	10	J	48	X-RAY DIFFRACTION	POSITIONAL	0.036
6	11	K	48	X-RAY DIFFRACTION	POSITIONAL	0.035
6	12	L	48	X-RAY DIFFRACTION	POSITIONAL	0.037
6	13	M	48	X-RAY DIFFRACTION	POSITIONAL	0.03
6	14	N	48	X-RAY DIFFRACTION	POSITIONAL	0.041
6	15	O	48	X-RAY DIFFRACTION	POSITIONAL	0.035
6	16	P	48	X-RAY DIFFRACTION	POSITIONAL	0.034
6	17	Q	48	X-RAY DIFFRACTION	POSITIONAL	0.03
6	18	R	48	X-RAY DIFFRACTION	POSITIONAL	0.033
6	19	S	48	X-RAY DIFFRACTION	POSITIONAL	0.03
6	20	T	48	X-RAY DIFFRACTION	POSITIONAL	0.039
7	1	A	16	X-RAY DIFFRACTION	POSITIONAL
7	2	B	16	X-RAY DIFFRACTION	POSITIONAL	0.017
7	3	C	16	X-RAY DIFFRACTION	POSITIONAL	0.023
7	4	D	16	X-RAY DIFFRACTION	POSITIONAL	0.021
7	5	E	16	X-RAY DIFFRACTION	POSITIONAL	0.015
7	6	F	16	X-RAY DIFFRACTION	POSITIONAL	0.021
7	7	G	16	X-RAY DIFFRACTION	POSITIONAL	0.035
7	8	H	16	X-RAY DIFFRACTION	POSITIONAL	0.014
7	9	I	16	X-RAY DIFFRACTION	POSITIONAL	0.013
7	10	J	16	X-RAY DIFFRACTION	POSITIONAL	0.023
7	11	K	16	X-RAY DIFFRACTION	POSITIONAL	0.027
7	12	L	16	X-RAY DIFFRACTION	POSITIONAL	0.02
7	13	M	16	X-RAY DIFFRACTION	POSITIONAL	0.015
7	14	N	16	X-RAY DIFFRACTION	POSITIONAL	0.024
7	15	O	16	X-RAY DIFFRACTION	POSITIONAL	0.047
7	16	P	16	X-RAY DIFFRACTION	POSITIONAL	0.017
7	17	Q	16	X-RAY DIFFRACTION	POSITIONAL	0.016
7	18	R	16	X-RAY DIFFRACTION	POSITIONAL	0.025
7	19	S	16	X-RAY DIFFRACTION	POSITIONAL	0.016
7	20	T	16	X-RAY DIFFRACTION	POSITIONAL	0.017
8	1	A	448	X-RAY DIFFRACTION	POSITIONAL
8	2	B	448	X-RAY DIFFRACTION	POSITIONAL	0.041
8	3	C	448	X-RAY DIFFRACTION	POSITIONAL	0.043
8	4	D	448	X-RAY DIFFRACTION	POSITIONAL	0.04
8	5	E	448	X-RAY DIFFRACTION	POSITIONAL	0.043
8	6	F	448	X-RAY DIFFRACTION	POSITIONAL	0.05
8	7	G	448	X-RAY DIFFRACTION	POSITIONAL	0.045
8	8	H	448	X-RAY DIFFRACTION	POSITIONAL	0.046
8	9	I	448	X-RAY DIFFRACTION	POSITIONAL	0.041
8	10	J	448	X-RAY DIFFRACTION	POSITIONAL	0.045
8	11	K	448	X-RAY DIFFRACTION	POSITIONAL	0.043
8	12	L	448	X-RAY DIFFRACTION	POSITIONAL	0.044
8	13	M	448	X-RAY DIFFRACTION	POSITIONAL	0.041
8	14	N	448	X-RAY DIFFRACTION	POSITIONAL	0.042
8	15	O	448	X-RAY DIFFRACTION	POSITIONAL	0.043
8	16	P	448	X-RAY DIFFRACTION	POSITIONAL	0.044
8	17	Q	448	X-RAY DIFFRACTION	POSITIONAL	0.043
8	18	R	448	X-RAY DIFFRACTION	POSITIONAL	0.043
8	19	S	448	X-RAY DIFFRACTION	POSITIONAL	0.043
8	20	T	440	X-RAY DIFFRACTION	POSITIONAL	0.039
9	1	A	24	X-RAY DIFFRACTION	POSITIONAL
9	2	B	24	X-RAY DIFFRACTION	POSITIONAL	0.038
9	3	C	24	X-RAY DIFFRACTION	POSITIONAL	0.027
9	4	D	24	X-RAY DIFFRACTION	POSITIONAL	0.045
9	5	E	24	X-RAY DIFFRACTION	POSITIONAL	0.031
9	6	F	24	X-RAY DIFFRACTION	POSITIONAL	0.04
9	7	G	24	X-RAY DIFFRACTION	POSITIONAL	0.023
9	8	H	24	X-RAY DIFFRACTION	POSITIONAL	0.026
9	9	J	24	X-RAY DIFFRACTION	POSITIONAL	0.059
9	10	K	24	X-RAY DIFFRACTION	POSITIONAL	0.028
9	11	M	24	X-RAY DIFFRACTION	POSITIONAL	0.03
9	12	N	24	X-RAY DIFFRACTION	POSITIONAL	0.042
9	13	O	24	X-RAY DIFFRACTION	POSITIONAL	0.026
9	14	Q	24	X-RAY DIFFRACTION	POSITIONAL	0.031
9	15	R	24	X-RAY DIFFRACTION	POSITIONAL	0.035
9	16	S	24	X-RAY DIFFRACTION	POSITIONAL	0.024
9	17	T	24	X-RAY DIFFRACTION	POSITIONAL	0.032
10	1	I	24	X-RAY DIFFRACTION	POSITIONAL
10	2	P	24	X-RAY DIFFRACTION	POSITIONAL	0.042
10	3	L	24	X-RAY DIFFRACTION	POSITIONAL	0.034
11	1	A	121	X-RAY DIFFRACTION	POSITIONAL
11	2	B	121	X-RAY DIFFRACTION	POSITIONAL	0.04
11	3	C	121	X-RAY DIFFRACTION	POSITIONAL	0.035
11	4	D	121	X-RAY DIFFRACTION	POSITIONAL	0.037
11	5	E	121	X-RAY DIFFRACTION	POSITIONAL	0.036
11	6	F	121	X-RAY DIFFRACTION	POSITIONAL	0.044
11	7	G	121	X-RAY DIFFRACTION	POSITIONAL	0.039
11	8	H	121	X-RAY DIFFRACTION	POSITIONAL	0.035
11	9	I	121	X-RAY DIFFRACTION	POSITIONAL	0.036
11	10	J	121	X-RAY DIFFRACTION	POSITIONAL	0.034
11	11	K	121	X-RAY DIFFRACTION	POSITIONAL	0.038
11	12	L	121	X-RAY DIFFRACTION	POSITIONAL	0.035
11	13	M	121	X-RAY DIFFRACTION	POSITIONAL	0.041
11	14	N	121	X-RAY DIFFRACTION	POSITIONAL	0.035
11	15	O	121	X-RAY DIFFRACTION	POSITIONAL	0.037
11	16	P	121	X-RAY DIFFRACTION	POSITIONAL	0.052
11	17	Q	121	X-RAY DIFFRACTION	POSITIONAL	0.042
11	18	R	121	X-RAY DIFFRACTION	POSITIONAL	0.044
11	19	S	121	X-RAY DIFFRACTION	POSITIONAL	0.037
11	20	T	121	X-RAY DIFFRACTION	POSITIONAL	0.039
12	1	A	63	X-RAY DIFFRACTION	POSITIONAL
12	2	I	63	X-RAY DIFFRACTION	POSITIONAL	0.041
12	3	R	63	X-RAY DIFFRACTION	POSITIONAL	0.061
13	1	B	63	X-RAY DIFFRACTION	POSITIONAL
13	2	C	63	X-RAY DIFFRACTION	POSITIONAL	0.039
13	3	D	63	X-RAY DIFFRACTION	POSITIONAL	0.042
13	4	E	63	X-RAY DIFFRACTION	POSITIONAL	0.036
13	5	F	63	X-RAY DIFFRACTION	POSITIONAL	0.046
13	6	G	63	X-RAY DIFFRACTION	POSITIONAL	0.04
13	7	H	63	X-RAY DIFFRACTION	POSITIONAL	0.038
13	8	J	63	X-RAY DIFFRACTION	POSITIONAL	0.045
13	9	K	63	X-RAY DIFFRACTION	POSITIONAL	0.042
13	10	L	63	X-RAY DIFFRACTION	POSITIONAL	0.048
13	11	M	63	X-RAY DIFFRACTION	POSITIONAL	0.042
13	12	N	63	X-RAY DIFFRACTION	POSITIONAL	0.036
13	13	O	63	X-RAY DIFFRACTION	POSITIONAL	0.04
13	14	P	63	X-RAY DIFFRACTION	POSITIONAL	0.039
13	15	Q	63	X-RAY DIFFRACTION	POSITIONAL	0.035
13	16	S	63	X-RAY DIFFRACTION	POSITIONAL	0.042
13	17	T	63	X-RAY DIFFRACTION	POSITIONAL	0.04
14	1	A	182	X-RAY DIFFRACTION	POSITIONAL
14	2	B	182	X-RAY DIFFRACTION	POSITIONAL	0.044
14	3	C	182	X-RAY DIFFRACTION	POSITIONAL	0.04
14	4	D	182	X-RAY DIFFRACTION	POSITIONAL	0.039
14	5	E	182	X-RAY DIFFRACTION	POSITIONAL	0.038
14	6	F	182	X-RAY DIFFRACTION	POSITIONAL	0.042
14	7	G	182	X-RAY DIFFRACTION	POSITIONAL	0.045
14	8	H	182	X-RAY DIFFRACTION	POSITIONAL	0.035
14	9	I	182	X-RAY DIFFRACTION	POSITIONAL	0.037
14	10	J	182	X-RAY DIFFRACTION	POSITIONAL	0.041
14	11	K	182	X-RAY DIFFRACTION	POSITIONAL	0.039
14	12	L	182	X-RAY DIFFRACTION	POSITIONAL	0.043
14	13	M	182	X-RAY DIFFRACTION	POSITIONAL	0.041
14	14	N	182	X-RAY DIFFRACTION	POSITIONAL	0.043
14	15	O	182	X-RAY DIFFRACTION	POSITIONAL	0.044
14	16	P	182	X-RAY DIFFRACTION	POSITIONAL	0.042
14	17	Q	182	X-RAY DIFFRACTION	POSITIONAL	0.047
14	18	R	182	X-RAY DIFFRACTION	POSITIONAL	0.041
14	19	S	182	X-RAY DIFFRACTION	POSITIONAL	0.042
14	20	T	182	X-RAY DIFFRACTION	POSITIONAL	0.035
15	1	A	25	X-RAY DIFFRACTION	POSITIONAL
15	2	C	25	X-RAY DIFFRACTION	POSITIONAL	0.035
15	3	D	25	X-RAY DIFFRACTION	POSITIONAL	0.029
15	4	E	25	X-RAY DIFFRACTION	POSITIONAL	0.021
15	5	F	25	X-RAY DIFFRACTION	POSITIONAL	0.023
15	6	G	25	X-RAY DIFFRACTION	POSITIONAL	0.031
15	7	H	25	X-RAY DIFFRACTION	POSITIONAL	0.032
15	8	I	25	X-RAY DIFFRACTION	POSITIONAL	0.02
15	9	J	25	X-RAY DIFFRACTION	POSITIONAL	0.037
15	10	K	25	X-RAY DIFFRACTION	POSITIONAL	0.034
15	11	L	25	X-RAY DIFFRACTION	POSITIONAL	0.025
15	12	N	25	X-RAY DIFFRACTION	POSITIONAL	0.025
15	13	O	25	X-RAY DIFFRACTION	POSITIONAL	0.027
15	14	Q	25	X-RAY DIFFRACTION	POSITIONAL	0.027
15	15	R	25	X-RAY DIFFRACTION	POSITIONAL	0.041
15	16	S	25	X-RAY DIFFRACTION	POSITIONAL	0.034
15	17	T	25	X-RAY DIFFRACTION	POSITIONAL	0.035
16	1	B	25	X-RAY DIFFRACTION	POSITIONAL
16	2	M	25	X-RAY DIFFRACTION	POSITIONAL	0.032
16	3	P	25	X-RAY DIFFRACTION	POSITIONAL	0.04
17	1	B	12	X-RAY DIFFRACTION	POSITIONAL
17	2	F	12	X-RAY DIFFRACTION	POSITIONAL	0.038
17	3	G	12	X-RAY DIFFRACTION	POSITIONAL	0.036
17	4	H	12	X-RAY DIFFRACTION	POSITIONAL	0.039
17	5	O	12	X-RAY DIFFRACTION	POSITIONAL	0.042
18	1	D	12	X-RAY DIFFRACTION	POSITIONAL
18	2	E	12	X-RAY DIFFRACTION	POSITIONAL	0.019
18	3	J	18	X-RAY DIFFRACTION	POSITIONAL	0.017
18	4	K	18	X-RAY DIFFRACTION	POSITIONAL	0.018
18	5	M	18	X-RAY DIFFRACTION	POSITIONAL	0.028
18	6	N	12	X-RAY DIFFRACTION	POSITIONAL	0.014
18	7	P	18	X-RAY DIFFRACTION	POSITIONAL	0.037
18	8	Q	18	X-RAY DIFFRACTION	POSITIONAL	0.025
18	9	R	18	X-RAY DIFFRACTION	POSITIONAL	0.025
18	10	T	18	X-RAY DIFFRACTION	POSITIONAL	0.046
19	1	C	15	X-RAY DIFFRACTION	POSITIONAL
19	2	I	15	X-RAY DIFFRACTION	POSITIONAL	0.023
19	3	L	15	X-RAY DIFFRACTION	POSITIONAL	0.029
19	4	S	12	X-RAY DIFFRACTION	POSITIONAL	0.029
20	1	A	135	X-RAY DIFFRACTION	POSITIONAL
20	2	B	135	X-RAY DIFFRACTION	POSITIONAL	0.043
20	3	C	135	X-RAY DIFFRACTION	POSITIONAL	0.043
20	4	D	135	X-RAY DIFFRACTION	POSITIONAL	0.041
20	5	E	135	X-RAY DIFFRACTION	POSITIONAL	0.039
20	6	F	135	X-RAY DIFFRACTION	POSITIONAL	0.048
20	7	G	135	X-RAY DIFFRACTION	POSITIONAL	0.043
20	8	H	135	X-RAY DIFFRACTION	POSITIONAL	0.04
20	9	I	135	X-RAY DIFFRACTION	POSITIONAL	0.044
20	10	J	135	X-RAY DIFFRACTION	POSITIONAL	0.041
20	11	K	135	X-RAY DIFFRACTION	POSITIONAL	0.048
20	12	L	135	X-RAY DIFFRACTION	POSITIONAL	0.044
20	13	M	135	X-RAY DIFFRACTION	POSITIONAL	0.05
20	14	N	135	X-RAY DIFFRACTION	POSITIONAL	0.045
20	15	O	135	X-RAY DIFFRACTION	POSITIONAL	0.047
20	16	P	135	X-RAY DIFFRACTION	POSITIONAL	0.062
20	17	Q	135	X-RAY DIFFRACTION	POSITIONAL	0.04
20	18	R	135	X-RAY DIFFRACTION	POSITIONAL	0.046
20	19	S	135	X-RAY DIFFRACTION	POSITIONAL	0.044
20	20	T	135	X-RAY DIFFRACTION	POSITIONAL	0.05

LS精密化 シェル

解像度 (Å)	Rfactor Rfree	Num. reflection Rfree	Rfactor Rwork	Num. reflection Rwork	Refine-ID	% reflection obs (%)
2.474-2.5021	0.3031	253	0.2467	5016	X-RAY DIFFRACTION	94
2.5021-2.5316	0.3007	267	0.2497	5268	X-RAY DIFFRACTION	98
2.5316-2.5624	0.3139	261	0.2453	5282	X-RAY DIFFRACTION	99
2.5624-2.5949	0.2751	271	0.2322	5274	X-RAY DIFFRACTION	99
2.5949-2.629	0.2784	294	0.2388	5324	X-RAY DIFFRACTION	99
2.629-2.665	0.2964	270	0.2401	5237	X-RAY DIFFRACTION	99
2.665-2.7031	0.2956	302	0.2319	5253	X-RAY DIFFRACTION	99
2.7031-2.7434	0.2597	294	0.2163	5305	X-RAY DIFFRACTION	99
2.7434-2.7863	0.2699	294	0.2164	5244	X-RAY DIFFRACTION	99
2.7863-2.832	0.2698	318	0.2239	5342	X-RAY DIFFRACTION	99
2.832-2.8808	0.2831	262	0.2137	5261	X-RAY DIFFRACTION	99
2.8808-2.9332	0.2475	258	0.2063	5350	X-RAY DIFFRACTION	99
2.9332-2.9896	0.262	286	0.2162	5261	X-RAY DIFFRACTION	99
2.9896-3.0506	0.241	257	0.2082	5375	X-RAY DIFFRACTION	99
3.0506-3.1169	0.2268	306	0.1993	5258	X-RAY DIFFRACTION	99
3.1169-3.1894	0.2187	276	0.1912	5375	X-RAY DIFFRACTION	99
3.1894-3.2692	0.2264	278	0.1895	5272	X-RAY DIFFRACTION	99
3.2692-3.3576	0.1995	273	0.1826	5396	X-RAY DIFFRACTION	100
3.3576-3.4563	0.2378	294	0.1886	5306	X-RAY DIFFRACTION	100
3.4563-3.5679	0.2173	293	0.1761	5345	X-RAY DIFFRACTION	100
3.5679-3.6954	0.2203	299	0.1672	5386	X-RAY DIFFRACTION	100
3.6954-3.8433	0.1939	287	0.1663	5345	X-RAY DIFFRACTION	100
3.8433-4.0181	0.2019	284	0.1604	5344	X-RAY DIFFRACTION	100
4.0181-4.2299	0.1827	267	0.155	5409	X-RAY DIFFRACTION	99
4.2299-4.4947	0.1948	277	0.1484	5375	X-RAY DIFFRACTION	99
4.4947-4.8415	0.1859	287	0.1557	5396	X-RAY DIFFRACTION	99
4.8415-5.3283	0.2102	285	0.1653	5387	X-RAY DIFFRACTION	99
5.3283-6.0983	0.2107	273	0.1892	5418	X-RAY DIFFRACTION	99
6.0983-7.6791	0.2321	282	0.203	5442	X-RAY DIFFRACTION	98
7.6791-51.5252	0.2371	278	0.2161	5565	X-RAY DIFFRACTION	96

精密化 TLS

手法: refined / Refine-ID: X-RAY DIFFRACTION

ID	L11 (°2)	L12 (°2)	L13 (°2)	L22 (°2)	L23 (°2)	L33 (°2)	S11 (Å °)	S12 (Å °)	S13 (Å °)	S21 (Å °)	S22 (Å °)	S23 (Å °)	S31 (Å °)	S32 (Å °)	S33 (Å °)	T11 (Å2)	T12 (Å2)	T13 (Å2)	T22 (Å2)	T23 (Å2)	T33 (Å2)	Origin x (Å)	Origin y (Å)	Origin z (Å)
1	-0.1686	-0.0489	0.1835	0.1927	-0.1437	0.3426	0.0221	-0.103	-0.1248	0.0368	0.0309	0.1832	-0.0344	-0.273	-0.0242	0.1186	0.0331	0.0055	0.1851	0.0209	0.1629	63.0622	99.7166	-10.5183
2	0.1462	0.0539	-0.0006	-0.0023	0.0026	-0.0391	0.1082	-0.0766	0.115	-0.005	-0.0137	0.1844	-0.0983	-0.0251	-0.1173	0.067	-0.0265	0.0312	0.1571	0.1128	0.1915	63.3871	76.3219	-7.6767
3	-0.2173	-0.1117	0.031	0.1274	-0.1116	0.1786	0.1093	0.062	0.2598	0.049	0.134	0.2915	-0.0299	-0.1945	-0.1913	0.0878	-0.0104	0.0819	0.2073	0.0842	0.2298	62.9629	72.0138	15.5116
4	0.2091	0.0115	0.0988	-0.0523	0.1063	0.0283	-0.0248	-0.0882	-0.1307	-0.0897	0.0501	0.0525	-0.1278	-0.1764	0.0174	0.1097	0.0939	-0.0101	0.1452	0.0362	0.0928	62.4041	92.5559	26.6344
5	0.0744	0.8363	0.4347	0.9418	0.5001	0.4561	0.1401	-0.0538	-0.1222	0.0339	-0.138	0.2747	0.1596	-0.1467	0.0283	0.1453	0.0326	-0.0413	0.1805	-0.0418	0.2139	62.4905	109.6447	10.5744
6	0.2197	-0.1089	-0.3349	-0.2052	0.0727	0.246	-0.0982	-0.1683	-0.1632	0.0633	-0.1012	0.0792	-0.0372	-0.2313	0.1887	0.0811	0.03	-0.0532	0.2055	-0.0348	0.2641	63.3853	175.7987	40.7473
7	0.1022	-0.046	0.0299	0.1465	0.0238	0.0157	0.076	-0.1788	0.0936	0.1379	-0.0243	-0.0071	0.0431	-0.0858	0.0129	0.0895	-0.1154	0.0266	0.1654	-0.0869	0.1331	63.7928	158.4824	24.873
8	0.4281	0.2513	-0.1291	0.1129	-0.1452	-0.0091	-0.1002	0.1265	0.1895	0.0187	0.0473	0.1668	-0.0179	-0.0186	-0.0173	0.1173	-0.0736	0.0285	0.0879	-0.0142	0.1588	63.6663	137.6701	35.4581
9	0.0822	0.1453	-0.2448	0.2595	-0.2328	0.3637	-0.0541	0.135	0.055	0.0063	0.0575	0.2106	0.0798	-0.313	-0.0138	0.0826	-0.0064	-0.0046	0.2432	-0.1288	0.2591	63.0231	141.7804	58.3345
10	-0.0165	0.0894	0.1542	0.1319	0.0084	-0.0482	0.1271	0.0956	-0.215	0.0335	-0.1853	0.0687	0.0344	-0.1565	0.0561	0.1549	0.1102	-0.1081	0.2062	-0.1214	0.3191	62.9732	165.2556	61.4265
11	0.0633	0.2535	0.2037	0.3945	0.0367	0.1446	0.0529	0.0942	-0.0209	-0.0236	0.1091	0.1565	-0.0122	0.0641	-0.0439	0.0294	-0.0435	-0.0251	0.0987	0.032	0.1551	62.9108	-0.2097	24.1143
12	-0.0109	-0.0786	0.0303	-0.0238	0.0774	0.2093	0.1135	0.0263	-0.0173	-0.0569	0.0119	0.0663	-0.0274	-0.0977	-0.0497	0.1608	0.0616	0.0342	0.1783	0.0341	0.139	62.4278	7.8752	45.9832
13	-0.4326	-0.2551	-0.0004	1.1628	0.6911	0.6295	-0.008	-0.1251	-0.2072	-0.0019	-0.1098	0.2989	0.0344	-0.1784	0.0592	0.0694	0.035	0.0351	0.192	0.0702	0.1703	62.5829	31.6304	45.1371
14	-0.5759	0.4201	-0.1279	0.4582	-0.2522	0.4013	0.0989	-0.2134	-0.069	-0.0217	0.1406	0.3054	0.1746	-0.3417	-0.1634	0.037	-0.0696	-0.0541	0.2814	0.0714	0.1338	62.9739	38.1164	22.974
15	0.5308	0.1743	-0.3045	1.2588	0.5988	0.3634	-0.0243	0.04	0.3997	0.1835	0.0025	0.1955	0.0557	-0.096	-0.0043	0.1063	-0.0046	-0.0588	0.0672	0.0204	0.2645	63.1965	18.3984	9.9746
16	0.0675	-0.314	-0.0912	0.3176	-0.0004	1.4394	0.2281	0.1856	-0.0834	-0.0491	-0.0919	0.1116	0.086	-0.3525	-0.1179	0.0582	0.0176	0.0141	0.1484	-0.0063	0.1771	62.6839	222.2098	86.4014
17	1.2115	0.3139	0.5906	0.3825	-0.0321	0.2773	-0.0609	-0.231	0.0173	-0.0736	0.0085	0.1508	-0.0096	-0.217	0.0057	0.067	0.0167	0.0463	0.1293	0.0327	0.1736	63.082	243.7965	77.1845
18	0.3857	0.6479	-0.6963	1.2988	-0.6018	1.457	0.1572	-0.0897	0.211	0.1084	0.0037	0.2202	-0.0319	-0.2508	-0.0413	0.1045	-0.0096	-0.0126	0.1888	-0.0497	0.1882	63.7698	241.6124	53.8158
19	0.1801	0.1744	-0.2642	0.1438	0.011	-0.0435	-0.0165	0.0836	0.1768	0.0851	-0.1062	0.1279	-0.0739	-0.2501	0.1258	0.0453	-0.0741	0.0114	0.2176	-0.072	0.1408	63.6968	218.8522	48.4786
20	-0.0467	0.1591	0.0934	0.3007	-0.0389	0.161	0.094	0.0799	0.3838	-0.0002	0.0357	0.0873	-0.0238	-0.2258	-0.1127	0.0776	-0.0339	0.0683	0.1929	-0.0275	0.1828	63.073	206.8724	68.7449
21	-0.0496	-0.047	-0.0693	-0.1194	-0.1179	0.2784	0.0319	0.0435	0.0377	-0.0555	0.1282	0.1449	-0.0059	-0.0733	-0.0462	0.0612	-0.0786	-0.0041	-0.0283	0.1058	0.1206	69.7228	81.7937	-15.0764
22	0.0222	-0.0063	-0.0662	0.0128	-0.01	0.0891	0.0604	-0.0542	-0.0192	0.0084	0.0418	0.0667	-0.03	-0.1185	-0.045	0.0351	-0.0075	0.0415	0.0611	0.0814	0.1024	69.5035	66.538	8.0173
23	0.2181	-0.1108	0.0383	0.1169	0.0649	-0.0424	0.0109	-0.0472	-0.1388	-0.0157	-0.1848	0.0173	0.0392	0.0031	0.0974	0.0955	0.0279	0.0521	0.0969	0.0691	0.2388	68.902	83.7594	29.8138
24	-0.1411	-0.0013	-0.0573	0.1477	-0.1433	0.0206	0.1119	-0.0467	-0.0474	-0.0234	0.0425	0.035	0.1197	0.0496	-0.0342	0.0274	0.0095	-0.035	0.111	-0.0624	0.0312	68.5922	109.8318	19.9193
25	0.0244	-0.0066	-0.0005	-0.0107	0.017	-0.017	0.0606	0.0352	-0.043	-0.0407	-0.0523	0.0483	0.0533	-0.01	0.0009	0.0773	0.0569	-0.0467	0.0744	-0.0564	0.1371	69.2115	108.5043	-7.7064
26	-0.0685	-0.164	-0.0198	1.2918	1.0577	1.1558	0.042	0.0794	0.0299	0.2379	-0.1548	0.101	0.2227	0.0135	0.0545	0.1292	-0.0504	0.0075	0.2275	-0.0443	0.066	70.0508	168.1387	24.2531
27	0.1321	0.1171	-0.0941	0.0259	-0.2055	-0.0949	0.1159	0.0242	-0.0293	0.0456	0.0055	0.1357	0.0413	0.0073	-0.0266	0.1635	-0.0512	-0.0666	0.0542	-0.0179	0.1411	70.2109	140.2613	26.6664
28	0.6991	-0.104	-0.1334	-0.072	0.0777	0.1621	0.2018	-0.1538	-0.0474	-0.054	-0.02	0.008	-0.2018	-0.06	-0.1155	0.226	-0.0581	-0.0251	0.1457	0.0064	0.0221	69.4854	133.9715	53.5001
29	0.0094	0.0849	-0.0935	0.0108	-0.0263	0.1515	0.0073	-0.1383	0.0744	-0.0434	-0.0096	0.1219	0.019	0.0234	0.0225	0.1222	0.0367	-0.048	0.2313	-0.0948	0.1152	69.1615	157.8548	67.4894
30	-0.0175	0.006	-0.0512	0.054	-0.0114	0.062	-0.0089	0.0593	0.0017	-0.0052	0.0178	0.0278	-0.0517	-0.1736	-0.0028	0.1747	0.06	0.0107	0.148	-0.0317	0.0231	69.536	179.0331	49.3511
31	0.1015	0.0655	-0.277	0.337	-0.2232	0.2904	-0.079	0.0771	-0.0404	-0.0655	0.0019	0.0317	-0.0272	-0.0089	0.0169	0.1173	-0.0978	-0.0629	0.1005	0.0319	0.0492	68.7502	-0.8669	42.4318
32	-0.0094	0.1451	-0.0196	-0.2503	0.1034	0.862	0.0516	0.0776	0.0536	0.093	0.0176	0.0291	0.1371	-0.0331	-0.0417	0.1584	0.01	-0.0113	0.2618	0.0906	0.0326	68.6427	25.2557	52.4108
33	0.106	0.0525	0.1306	-0.0485	0.1856	0.1368	0.1205	-0.0362	-0.0321	0.0077	0.0943	0.0603	0.1192	-0.2703	-0.0725	0.1199	-0.0099	-0.0559	0.0959	0.0853	-0.0426	69.2078	42.9344	31.0237
34	0.0298	-0.0286	-0.0334	0.0342	0.0632	0.0184	0.0418	0.0279	-0.097	-0.0788	-0.0887	0.1325	-0.0405	-0.0325	0.0164	0.1764	0.0109	-0.1296	0.006	0.0075	0.2585	69.5316	27.601	7.9593
35	0.2268	0.0432	-0.0302	-0.2408	-0.0359	0.2737	0.1086	-0.0804	-0.131	-0.0102	0.0729	0.1245	-0.0795	-0.0202	-0.0737	0.0254	-0.082	-0.0065	-0.0113	0.0867	0.2041	69.3638	0.5991	14.9196
36	-0.1276	0.1542	0.0013	-0.2572	0.0216	-0.0009	-0.0067	-0.0312	-0.0425	0.0061	0.0436	0.1171	0.0219	-0.0148	0.0058	0.0614	0.2441	0.0101	0.0068	0.0443	0.0826	69.0345	240.7142	86.1424
37	0.8149	0.1966	-0.315	-0.2702	-0.0419	1.0348	0.2073	0.087	0.1939	0.0139	0.0799	0.0158	-0.0805	-0.0037	-0.1807	0.0507	0.0071	0.0619	0.0342	-0.0256	0.1379	69.8845	249.1413	59.7483
38	0.0872	0.1243	0.119	0.0605	-0.0196	0.195	0.0798	0.0599	-0.0668	0.1253	-0.0434	-0.0297	0.0155	-0.0319	0.0064	0.0764	-0.077	-0.073	-0.0721	-0.1205	0.0455	70.1949	226.5701	43.3825
39	-0.0803	-0.1613	0.0242	-0.0863	0.1801	0.0964	0.0097	0.1305	0.0787	-0.0549	0.1763	0.0408	-0.033	-0.3114	-0.0956	0.0885	-0.0989	0.0765	0.1894	0.0216	-0.0064	69.9264	205.8137	61.2335
40	0.079	-0.0696	-0.0909	0.223	0.0031	0.005	0.0087	-0.009	-0.0387	-0.0622	-0.0489	0.039	-0.0386	-0.0644	0.0365	0.0859	-0.0013	0.1055	0.0851	-0.1014	0.0363	68.8843	212.8741	86.418
41	0.5045	0.2051	-0.0762	0.1986	0.0137	0.2623	0.1593	0.0985	0.0552	-0.0612	-0.1046	-0.1454	-0.0132	0.0782	0.0972	0.0458	0.0293	0.0667	0.0708	0.0441	0.1421	93.1993	89.3673	-14.1526
42	0.6454	-0.1424	0.1358	0.6311	0.0484	0.1146	0.1404	-0.095	-0.1342	-0.0044	-0.0924	-0.1286	0.0982	0.0068	0.1231	0.0546	0.019	-0.004	0.0538	0.0629	0.1028	93.2357	69.6594	1.8333
43	1.6477	-0.0107	0.3097	0.3847	-0.2658	0.3443	0.2185	-0.0919	0.1085	-0.0162	-0.0634	0.0117	0.1437	-0.0204	-0.028	0.0378	0.0438	0.0038	0.0392	0.0596	0.1496	92.7068	78.8294	25.3973
44	0.0351	-0.0981	0.2173	0.1627	0.0048	0.246	0.019	-0.1389	0.1873	0.0233	-0.0553	-0.0936	-0.052	-0.0322	0.011	0.0369	-0.0287	0.0163	0.067	-0.0025	0.1838	92.2813	104.1459	24.1392
45	0.1988	0.074	0.0468	0.4553	0.0398	0.2446	0.0372	0.061	0.1905	-0.0853	-0.0773	-0.0964	-0.0817	0.1208	0.0565	0.0986	-0.006	0.0456	0.0936	0.0101	0.1687	92.5899	110.6173	-0.2018
46	0.6649	-0.261	-0.2633	0.2413	0.108	0.3481	0.0991	0.131	0.0831	-0.0675	-0.0346	-0.1037	-0.0169	0.0818	-0.0434	0.0534	-0.0021	0.0221	0.0977	-0.0613	0.1315	93.5795	172.3613	30.5611
47	0.1702	0.2069	0.2627	-0.0697	0.0376	0.2943	0.0276	-0.0252	-0.0963	-0.1162	0.0666	-0.215	0.0719	0.0492	0.0346	0.0315	0.0099	0.0265	0.0803	-0.1302	0.2452	93.9541	147.3652	25.4059
48	0.128	0.0586	-0.2332	0.1279	0.0023	0.1019	0.0586	-0.1106	-0.0759	0.1002	-0.0184	-0.1264	0.0707	0.0656	-0.1385	0.0507	-0.0058	-0.0906	0.1085	-0.0919	0.2436	93.3624	134.2029	46.9604
49	0.3398	0.0063	0.0458	0.2904	0.3353	0.7341	0.1475	-0.0931	-0.0607	0.1415	0.0816	-0.1966	0.1619	0.1899	-0.2291	0.0807	0.011	-0.0756	0.0615	-0.0482	0.1798	92.817	151.0797	65.7234
50	0.2826	-0.0125	0.2206	0.3295	0.044	0.3016	0.0143	0.0948	-0.0061	0.0593	-0.1114	-0.1143	-0.0969	0.113	-0.2209	0.028	-0.0601	-0.0426	0.045	-0.1331	0.0381	93.1387	174.4562	55.5403
51	1.5533	0.0732	-0.6101	0.7407	-0.2379	0.3051	0.0544	-0.3163	-0.2714	-0.0928	-0.0946	-0.0701	0.0318	0.1114	0.2186	0.0411	-0.0045	-0.0046	0.0966	0.0615	0.0797	92.6101	-1.8686	35.7782
52	0.9111	0.0288	-0.004	0.6243	-0.3554	0.6461	0.2457	0.0673	0.043	0.18	-0.104	-0.0681	-0.0284	0.0909	0.1496	0.0829	-0.008	-0.0389	0.0663	0.0478	0.1029	92.2987	17.9495	51.4848
53	1.3163	0.0281	-0.0508	0.5765	0.0149	0.2738	0.2069	0.0399	0.1045	0.0564	-0.0984	-0.1482	-0.0732	0.0403	0.1968	0.0543	-0.027	-0.0045	0.0704	0.0185	0.0369	92.7027	39.3208	37.7398
54	0.3119	0.0742	0.1631	0.5624	-0.0671	0.1946	0.0072	0.0514	-0.0712	-0.2164	0.1142	-0.0318	-0.063	0.0294	0.041	0.0888	-0.0452	0.0274	0.0485	-0.0016	0.0723	93.1765	32.4658	13.3725
55	0.913	0.0684	0.2761	0.6527	-0.0103	0.3021	0.0117	0.0221	-0.2542	-0.2571	-0.0142	-0.158	-0.043	-0.0764	0.0463	0.0879	-0.0403	0.0507	-0.0103	0.0101	0.0545	93.0573	7.1244	12.1757
56	0.6098	-0.3007	0.0864	0.2443	-0.0688	0.219	-0.0303	-0.0322	0.1374	0.1073	-0.0136	-0.081	0.0229	0.0852	-0.0704	0.0676	-0.0048	-0.0203	0.0115	-0.0131	0.0339	92.5665	233.6183	88.3594
57	2.1958	-0.5695	-0.3089	0.4509	0.0992	0.276	0.0757	0.3059	0.0254	-0.016	-0.1219	-0.0937	-0.1211	0.0329	0.1189	0.0333	-0.0088	0.0238	0.0507	0.0107	0.0332	93.324	248.1345	67.591
58	0.5594	0.1284	0.076	0.1845	-0.0318	0.1479	0.0681	0.133	-0.0757	-0.0949	0.0048	-0.072	-0.0263	0.0496	0.0171	0.0421	-0.0105	0.0267	0.0419	-0.0133	0.0676	93.8168	233.0503	47.3005
59	0.7869	0.1225	-0.3063	0.3017	0.0374	0.3669	0.1639	-0.0952	-0.0704	-0.0554	-0.1376	-0.0902	0.1115	0.0933	0.1095	0.0454	0.0271	0.0026	0.066	-0.0037	0.0593	93.4744	209.2098	55.5058
60	0.4623	0.0119	-0.0306	0.3878	0.0546	0.1748	0.1418	-0.0041	-0.0591	0.0359	-0.1179	-0.0741	0.1351	0.0401	-0.1233	0.0658	-0.0132	-0.0012	0.0113	-0.0613	0.0663	92.6455	209.4003	80.9093
61	5.0536	4.6734	-7.4364	-1.266	-3.2285	4.5494	0.0437	0.0502	-0.0064	-0.117	-0.0403	-0.0074	-0.0471	-0.072	-0.0046	0.5787	-0.0535	-0.0237	0.5608	-0.0099	0.4578	67.0322	88.7793	-23.0388
62	8.6807	0.1442	0.785	4.2794	3.9443	3.3016	-0.0386	0.0624	-0.058	0.3011	0.0626	0.1746	0.3036	0.1629	-0.01	0.7343	0.0352	0.2656	0.4275	-0.0207	0.5809	67.3339	60.988	-1.0501
63	3.6319	-4.032	5.4304	3.5599	0.4602	3.5229	0.0765	0.0364	0.0739	0.1016	-0.0695	-0.0883	-0.0534	-0.0819	-0.0123	0.2345	0.2056	0.0207	0.7208	0.2679	0.4957	66.3983	73.5713	32.1898
64	-0.0458	2.0018	2.8459	3.5743	3.7371	3.7169	0.1307	-0.1286	0.0629	0.1821	-0.0424	0.0613	0.2438	0.0882	-0.0865	0.3852	0.0279	-0.1322	0.4705	-0.229	0.5529	65.9682	108.8955	30.4449
65	-0.91	7.2687	-1.8953	4.6449	-9.3182	3.7565	0.0861	0.0638	0.0207	0.1487	0.0127	-0.0287	-0.0952	-0.0282	-0.0749	0.5018	0.0831	-0.1539	0.4905	-0.041	0.549	66.5019	118.4312	-3.4659
66	-0.2551	2.9548	-9.333	4.1446	0.0139	3.6103	0.1635	0.0278	0.0101	0.2609	-0.0327	-0.0776	-0.1489	-0.0542	-0.1153	0.5436	-0.2301	-0.3038	0.4866	0.1547	0.5088	67.5	178.9123	24.6051
67	-0.6553	-5.1137	0.9481	2.8648	3.4278	4.1688	0.0585	0.0458	-0.0227	-0.1341	-0.0851	0.0202	-0.1593	0.0221	0.0063	0.6806	-0.4454	0.0274	0.5818	-0.0681	0.2965	67.898	143.9427	16.9636
68	5.2302	-7.0179	-3.6214	4.8055	0.6328	1.295	0.0137	-0.0213	-0.1748	0.0062	0.0842	0.0228	-0.021	0.0751	-0.0809	0.4791	-0.028	0.1156	0.4149	-0.1192	0.5858	67.1627	125.6292	46.8405
69	3.3074	1.4207	7.9333	3.1335	0.8765	3.7693	-0.0078	0.0659	0.0439	0.1209	-0.1033	-0.0345	-0.1638	-0.1539	0.1131	0.497	0.1544	-0.1307	0.5323	-0.0556	0.5431	66.3948	148.9979	73.3145
70	-3.3776	5.3719	1.9982	3.9403	4.1119	3.9767	0.0268	-0.0732	0.0547	0.0131	-0.0592	0.057	-0.2554	0.1813	0.0414	0.4528	0.0016	-0.2803	0.4191	-0.1379	0.3948	66.6189	181.6023	59.698
71	2.7412	-9.7805	1.9935	3.8787	-8.7881	3.6984	0.032	-0.0198	-0.0726	-0.1038	0.0594	0.0191	0.0668	0.0017	-0.0557	0.4502	0.1648	0.2989	0.3492	-0.0598	0.5382	66.4543	-10.179	37.652
72	5.2902	-8.8595	3.9543	7.3301	0.7137	3.9059	-0.0196	-0.0067	0.1055	0.0715	-0.1076	-0.0926	-0.0987	-0.0258	0.1298	0.5628	0.1827	-0.0058	0.5856	0.1445	0.5579	65.926	17.4152	59.6524
73	-1.3947	5.1523	2.6803	4.8367	4.2977	3.6002	0.1156	-0.0848	0.0233	-0.2064	0.0528	0.0259	-0.3397	0.1935	-0.1289	0.5757	-0.2188	-0.2066	0.4454	-0.1739	0.3997	66.3223	47.5846	40.322
74	-0.5668	3.0324	-5.8147	3.6414	0.4355	3.751	0.0513	-0.0029	-0.031	-0.0789	0.0797	0.0219	0.0254	-0.1494	-0.1302	0.3835	-0.2461	-0.1035	0.5412	0.2857	0.6241	67.145	37.9854	6.4038
75	-0.7136	1.0023	0.859	3.952	4.4925	4.9771	0.1527	0.0901	-0.011	-0.5385	-0.0056	0.0247	-0.4928	0.1789	-0.1574	0.4735	-0.1767	0.1216	0.5499	-0.146	0.3447	66.9465	2.623	4.6417
76	-2.074	5.264	3.2141	2.7872	5.4704	2.6143	0.0428	-0.0429	0.0117	0.081	0.0556	0.0097	-0.0077	-0.0176	-0.0924	0.3636	0.0572	-0.2125	0.3024	0.1185	0.2499	67.1946	256.7719	66.9744
77	2.6753	-5.8989	-8.6474	4.2831	4.385	4.3415	0.1547	-0.0731	0.1107	0.0102	-0.0481	0.0795	0.0999	0.0688	-0.0737	0.4451	-0.0815	0.2335	0.5388	-0.1221	0.587	67.3376	202.2137	49.6429
78	6.0844	0.7502	1.9999	3.8798	0.0908	3.7811	0.037	0.0172	-0.0636	-0.0936	-0.0562	-0.097	0.2078	0.0358	0.024	0.4318	0.2701	0.2704	0.2688	0.2157	0.4816	66.3295	202.4025	85.0024
79	-3.0031	-0.2876	1.5878	3.4663	0.9952	3.5028	-0.1476	-0.2456	0.0448	-0.0769	-0.0677	0.027	-0.4428	-0.4773	0.202	0.45	0.436	0.0549	0.4037	-0.0077	0.2423	65.6898	235.8681	95.5934
80	-2.2092	7.523	-5.8437	7.4732	-3.6001	9.5306	-0.0702	0.4614	0.2261	-0.107	-0.0037	-0.2299	0.3189	-0.2807	0.0697	0.4511	-0.2193	-0.1472	0.5387	0.1847	0.4359	67.2817	236.3593	38.6229
81	0.1299	-0.0833	0.0292	0.0275	0.1613	0.4247	0.1026	-0.0069	-0.0819	-0.1686	0.0009	0.0246	-0.0574	-0.0391	0.0691	0.2075	-0.0232	-0.0571	0.1048	-0.0491	0.0544	64.1572	95.9407	-19.7726
82	-0.023	-0.0369	0.0694	0.1775	-0.0645	0.0732	0.0055	-0.0099	-0.0059	-0.1042	-0.0541	0.0551	0.1093	-0.0195	-0.0096	0.1228	-0.0217	0.0496	0.0573	0.0584	0.1291	64.4867	66.2143	-6.9471
83	0.0597	0.0156	0.0803	0.1648	-0.111	0.1631	-0.0074	-0.0679	0.0066	-0.0236	0.0348	0.0819	0.0646	-0.0601	-0.0236	0.1148	0.0297	0.0152	0.1541	0.0352	0.1022	63.9443	69.4985	25.1879
84	-0.1136	0.052	0.0966	0.0434	0.0478	0.1139	0.0113	-0.1566	0.1951	0.0091	-0.0405	0.0881	0.0316	-0.1283	0.0266	-0.0139	-0.0316	-0.0786	0.1531	-0.0018	0.1896	63.3477	101.0588	32.0353
85	0.3079	0.1888	-0.0351	0.0544	-0.0004	0.4625	0.0045	0.0584	0.1968	0.1251	-0.0608	0.1159	-0.27	0.0385	0.0218	0.1584	-0.0199	-0.0172	0.1114	0.0457	0.1566	63.5095	117.429	4.2057
86	0.1985	-0.1797	-0.1563	0.3892	0.2493	0.1108	0.0599	0.2538	-0.0875	-0	-0.1165	0.0659	-0.0817	-0.0238	0.0947	0.1076	0.0195	-0.1081	0.1868	-0.1066	0.1609	64.6527	180.7915	32.0732
87	0.3285	0.2546	-0.6338	0.1964	-0.4088	0.9261	-0.1145	0.131	-0.0411	-0.0985	0.1473	-0.0051	0.0139	-0.2128	-0.0217	0.0352	-0.1463	0.1455	0.2019	0.0078	-0.0203	65.1732	151.9717	17.4802
88	0.1479	-0.2255	-0.011	0.4405	0.0704	0.1051	0.0317	0.0536	-0.2137	-0.034	-0.069	0.1694	-0.0138	-0.0341	0.0265	0.1767	0.0247	-0.0445	0.1637	-0.0132	0.2998	64.6701	128.5562	39.429
89	0.1827	-0.0181	0.0799	0.1498	-0.0142	0.0915	0.1048	-0.0977	-0.1255	0.0474	0.0386	-0.045	0.0534	-0.0393	-0.0476	0.081	-0.0519	-0.0341	0.0316	0.0537	0.2035	63.8158	142.994	68.234
90	0.0197	-0.0037	-0.0062	0.0394	0.0106	0.1021	0.0664	0.052	0.0037	0.0293	0.0317	0.003	0.0444	-0.0099	-0.0201	0.1306	0.0228	-0.0889	0.0567	-0.0134	0.0943	63.9537	175.0289	63.6181
91	0.2903	-0.2545	0.1827	0.2383	-0.1715	0.1116	0.0149	-0.1131	-0.1365	-0.0424	0.0209	0.2009	0.0501	-0.0314	-0.083	0.0601	0.0289	-0.0354	0.0695	0.038	0.1443	63.8338	-8.6302	29.5982
92	0.0312	-0.022	-0.0323	0.0133	0.0051	-0.0277	-0.0472	0.0093	-0.0138	0.1494	0.0353	0.0519	0.0493	-0.0202	0.0127	0.1998	0.0603	0.0821	0.0628	-0.0321	0.0159	63.3431	10.5495	55.6643
93	0.4766	-0.5909	0.1535	0.7986	-0.2198	0.1326	-0.1676	-0.0643	0.1071	0.2622	0.1573	-0.0102	-0.0634	-0.0815	-0.0423	0.0912	0.1135	-0.0264	0.1101	0.0982	0.1197	63.6591	41.5538	45.6662
94	0.0632	0.1934	-0.0662	0.2246	-0.1347	0.0722	-0.043	0.1074	0.1231	0.0064	0.0782	0.1136	0.0099	-0.0501	-0.0636	0.0753	-0.0314	-0.0117	0.182	0.0474	0.119	64.2614	41.377	13.4601
95	0.0729	0.1436	-0.0049	0.1506	0.0519	-0.0182	-0.0505	0.0508	-0.0118	-0.2432	0.1233	0.0616	0.0628	-0.0334	-0.0392	0.1679	-0.1184	-0.1202	-0.0892	0.0556	0.2524	64.1955	10.572	3.8099
96	-0.0006	0.0073	-0.0154	0.034	0.0353	0.1098	0.0058	-0.0237	0.0169	0.0404	0.0357	-0.0182	0.0763	0.0347	0.0213	0.0619	0.057	0.0149	0.0145	-0.0492	0.0512	63.3802	228.4152	94.217
97	0.0827	-0.0487	-0.0167	0.1267	0.0374	0.1644	0.0078	0.0433	0.0361	0.0285	-0.027	0.076	-0.0184	0.001	0.0005	0.1647	0.0159	-0.0439	0.0882	-0.0161	0.0553	64.1823	253.3005	73.7526
98	0.2138	0.1325	0.0631	0.0435	0.0469	-0.0002	0.0312	-0.0366	0.0593	-0.0361	0.0404	0.0466	0.0212	-0.0704	0.0021	0.0857	-0.1001	-0.0488	0.1123	-0.0352	0.157	65.0545	241.4452	43.9111
99	0.0492	-0.0081	-0.0074	0.0021	0.0016	0.023	0.0022	0.0016	0.0055	-0.0188	-0.0172	-0.0056	0.0241	-0.0814	0.0122	0.0304	-0.1402	0.0596	0.119	-0.0416	0.0982	64.8703	209.2891	45.8003
100	0.0018	-0.1147	-0.0427	-0.1847	0.0094	0.1579	-0.0207	0.0009	-0.0336	0.0687	-0.0672	0.0703	0.1696	-0.1813	0.0904	0.073	-0.1453	0.0784	0.1034	-0.0791	0.0433	63.8404	201.1879	77.0608
101	0.6002	-1.5223	-0.2221	0.7589	-0.1441	-0.0728	0.0651	0.0052	0.0144	-0.0874	-0.0908	-0.0076	-0.0395	-0.0808	0.029	0.3019	0.2376	-0.095	0.5106	-0.1238	0.3589	59.827	106.1343	-24.3234
102	-0.1414	-0.2535	0.5219	-0.0407	0.0869	0.3606	-0.0211	-0.0121	0.0335	-0.0241	0.0006	0.0091	0.0055	0.0488	0.0169	0.2575	0.0108	-0.3146	0.3727	-0.0603	0.5674	60.5172	65.0513	-18.1708
103	-0.2803	-0.0234	-0.13	0.1496	0.0306	-0.0551	0.0179	-0.0079	0.0055	-0.0093	0.0253	0.0218	0.0203	-0.05	-0.0351	0.2492	-0.1734	-0.1281	0.5998	0.1019	0.5738	59.9565	58.4797	22.8533
104	0.2115	0.1737	0.3398	0.156	-0.181	-0.0116	0.0522	-0.1173	0.101	0.0317	-0.0403	0.1023	0.0052	-0.0645	-0.0006	0.2899	-0.0661	0.0295	0.5208	0.104	0.37	58.7917	95.4769	41.2838
105	0.7471	0.2653	0.0905	0.5607	-0.2157	0.4768	0.0557	-0.0248	0.1977	0.0073	0.0075	0.0008	-0.0878	-0.0374	-0.0634	0.5082	0.2857	0.1685	0.5018	0.0134	0.5835	59.0508	124.9048	12.3821
106	1.6453	-0.3566	-1.0861	0.1274	0.7327	0.5989	0.0427	0.1116	0.0065	-0.06	-0.0979	0.0215	-0.0411	-0.0505	0.0644	0.3933	0.3178	0.0536	0.6104	-0.1729	0.5329	60.3589	190.7076	37.0893
107	-0.5134	-0.557	-0.5517	-0.8466	-0.7179	1.0184	0.0694	0.1871	-0.1969	-0.0345	0.017	-0.1071	-0.1526	-0.3315	-0.11	0.2778	0.128	0.0776	0.4748	0.1616	0.4689	60.8901	159.8702	9.8711
108	0.0094	0.1669	0.0913	0.2099	0.212	0.5516	0.0647	0.0207	-0.1508	-0.0344	-0.0297	0.0987	-0.0054	-0.0037	-0.0296	0.5636	-0.1811	-0.3254	0.7372	0.0217	0.7731	60.7106	123.5998	29.3897
109	-0.0801	0.7385	-0.0878	0.0948	1.1175	-0.6794	0.0899	-0.0145	-0.1354	0.0147	0.0124	-0.1428	0.0267	-0.0176	-0.098	0.5641	-0.1347	0.0233	0.5354	-0.1585	0.5868	59.5971	131.9325	69.8446
110	0.1054	-0.0551	0.3529	0.1325	-0.013	-0.0399	0.0274	0.0137	-0.0491	-0.0031	-0.0079	0.0206	-0.0038	0.0048	-0.001	0.3987	-0.0262	0.1454	0.4786	-0.0801	0.6063	59.4806	173.0629	74.5812
111	-1.7603	1.0871	0.738	0.9687	0.6464	-0.1755	0.081	-0.174	-0.1335	-0.0973	0.0175	0.0914	0.0545	0.0014	-0.0973	0.4475	-0.1228	-0.1152	0.5372	0.0392	0.6429	59.8879	-15.3555	20.6336
112	-0.3787	1.4013	-0.0857	1.0626	-0.2907	-0.026	0.0265	-0.067	-0.1019	0.0502	-0.0798	-0.0206	-0.0487	0.0531	0.0432	0.6378	-0.3305	0.0098	0.6648	0.1099	0.769	59.1096	-0.1274	59.0796
113	0.4587	0.2337	-0.0274	0.3814	-0.631	1.1154	-0.0228	-0.1042	-0.0053	0.0546	0.0809	0.0212	-0.0627	-0.0621	-0.0602	0.4003	-0.0235	0.2516	0.4766	0.0039	0.4098	59.1727	41.6043	56.762
114	-0.0484	0.2987	0.006	0.3576	0.37	-0.1114	-0.004	0.0111	0.0304	0.0498	0.1189	0.1751	-0.0415	-0.1005	-0.1091	0.4326	0.1703	0.1197	0.6233	0.0327	0.6555	60.0971	52.1521	16.8078
115	-0.1005	0.2226	0.6367	0.1896	0.2247	0.3719	-0.0479	0.0197	0.0321	-0.1381	0.0834	0.0887	0.0364	0.0696	-0.037	0.9371	0.0568	-0.1167	1.0546	0.0288	0.9636	60.0916	17.6344	-5.0708
116	-0.8277	-0.6619	-0.5551	0.4397	0.2087	-0.2375	-0.006	-0.0603	0.0427	-0.0183	-0.0165	0.0564	0.011	-0.0164	0.0178	0.3629	-0.0457	0.173	0.4656	-0.1108	0.5844	59.0011	219.9076	101.5363
117	-0.2214	0.1844	-0.1002	0.2828	0.0793	0.1492	0.0124	0.0222	0.0686	-0.0139	-0.0126	-0.0117	0.0033	-0.063	0.0042	0.3695	0.2744	-0.1555	0.5555	0.0595	0.5297	60.6537	252.448	43.1546
118	0.1706	-0.4907	0.6683	0.0541	-0.1386	-0.0198	-0.026	-0.0383	0.0583	-0.0169	-0.0147	-0.0067	-0.0016	-0.0177	0.0425	0.5115	0.1449	-0.2856	0.6381	-0.0042	0.619	61.0413	211.7753	34.8084
119	-0.1659	0.3624	0.2922	-0.0726	0.5839	0.7971	-0.0115	0.001	0.0462	0.0548	-0.0747	0.0372	0.0574	-0.1106	0.0853	0.4446	-0.5077	-0.0431	0.6223	-0.2695	0.4727	59.7809	191.8483	70.9694
120	0.1147	-0.057	0.0091	0.3015	-0.1186	0.0681	0.0561	0.1643	0.0494	-0.1413	-0.0833	-0.1664	0.0289	-0.0122	0.057	0.0717	0.0711	0.0251	-0.1473	0.1392	-0.0009	84.5775	90.9811	-11.8375
121	0.0717	0.0103	0.0098	0.1746	0.0332	0.0455	-0.0093	0.0258	0.0727	-0.0043	0.0298	-0.0047	0.0477	0.0379	0.187	0.0826	0.0248	0.0168	0.0318	0.0537	0.0877	84.6165	72.3465	0.7627
122	-0.0378	-0.1937	0.0645	-0.0021	-0.0434	0.0708	0.0183	-0.0715	0.1595	0.0446	0.0285	-0.0382	-0.0255	0.0034	0.1923	0.0669	0.0041	-0.0088	0.0203	0.0851	0.0541	84.1565	78.6706	22.2914
123	0.1423	-0.016	0.0788	0.5768	0.1734	0.1189	0.0708	-0.023	0.1044	-0.0431	-0.0575	0.0242	-0.0337	-0.0202	-0.0142	0.0186	-0.0132	0.0013	0.03	-0.0083	0.0612	83.7948	101.1444	23.0488
124	0.3096	0.0762	-0.1315	0.2239	0.0493	0.1151	0.0005	-0.0431	0.2541	-0.1229	0.0016	-0.0739	-0.1746	0.0387	-0.0819	0.0761	0.0443	0.0399	-0.1052	0.0378	0.0949	84.033	108.7134	1.9988
125	1.3656	-0.6872	-0.3119	0.5026	0.4098	0.2289	-0.0284	0.227	0.1525	-0.0439	-0.002	-0.1401	-0.0173	-0.0425	-0.1051	0.0637	0.0206	0.0413	0.0352	-0.0247	0.0408	85.018	171.4709	33.2408
126	0.0865	-0.0529	-0.2794	0.8257	0.6382	0.5215	0.1835	0.1915	-0.1015	-0.0449	0.0915	-0.0795	0.0165	-0.2166	0.2935	0.0165	-0.0283	0.0151	-0.0894	-0.2113	0.0003	85.2976	149.7953	26.8774
127	0.1749	0.0314	0.0965	0.7036	0.262	0.1921	-0.0462	-0.0986	-0.1868	0.0918	0.055	-0.0584	-0.0786	0.0759	0.0343	0.0595	-0.0331	-0.0766	-0.3253	-0.1629	0.0955	84.8527	136.5775	44.9198
128	0.3831	0.3368	0.175	0.4326	0.169	0.1592	0.0625	-0.1051	-0.0955	0.138	-0.0319	-0.165	-0.0412	-0.0096	-0.0177	0.0873	0.002	-0.0791	0.0437	-0.0305	0.0923	84.3378	150.0548	62.667
129	0.1714	0.0633	-0.0902	0.1713	0.0989	0.1456	0.0798	-0.0149	-0.0073	-0.0325	0.0348	0.07	-0.0766	0.0003	0.3844	0.0579	0.0059	-0.0221	0.0542	-0.0911	0.0618	84.4987	171.5084	55.4483
130	0.1446	-0.0758	0.011	0.7345	-0.5161	0.3626	0.0449	-0.229	-0.1937	-0.0069	0.0149	0.0123	0.0199	0.1816	0.0393	0.0313	-0.0109	-0.007	-0.1405	0.0699	0.0445	84.0893	0.1011	33.417
131	0.2678	0.0351	0.1348	0.127	0.0774	-0.0025	0.0282	-0.2094	-0.028	0.116	-0.0789	-0.101	-0.0436	0.0528	-0.1761	0.0857	-0.0592	-0.0212	0.0401	0.0769	0.0015	83.7771	16.4964	48.8285
132	0.0993	-0.214	-0.0309	0.2215	0.046	0.0951	0.0538	-0.0949	0.1321	-0.0151	0.02	-0.0568	-0.0773	0.0286	0.1296	0.0653	-0.0264	0.024	0.0085	0.0289	0.0029	84.1101	36.4554	38.2096
133	0.0485	0.101	-0.1802	0.4564	-0.137	0.4198	-0.0282	0.0749	-0.0209	-0.1803	0.111	0.0186	0.0806	-0.0311	0.1608	0.0696	0.0064	0.0148	0.0002	0.0412	0.0232	84.5272	32.2324	16.1981
134	0.4457	0.2722	-0.0803	0.2108	-0.0681	0.0648	-0.091	0.014	-0.1067	-0.1383	0.0483	-0.041	0.0513	0.0037	-0.0376	0.1381	-0.0184	-0.0171	0.0158	0.0063	0.0175	84.4812	9.8885	13.2725
135	0.1969	0.1785	-0.153	0.455	-0.3206	0.1813	0.0258	-0.0776	-0.0147	-0.1131	-0.0962	-0.0419	0.0344	0.0798	-0.1121	0.0828	-0.0133	0.0085	-0.0274	-0.0345	-0.0049	84.0801	231.2474	86.2361
136	0.181	0.0995	-0.0779	0.1448	-0.0448	0.3436	-0.0029	0.0906	0.0003	0.0271	0.0118	0.0459	-0.0254	0.1217	0.1683	0.0618	-0.0074	0.027	-0.0433	0.019	0.0298	84.6576	245.7028	68.9524
137	0.1267	0.0256	-0.0447	0.2403	0.0487	0.1871	0.0425	0.0558	0.0364	0.019	-0.0465	-0.0702	0.0732	-0.0166	-0.0322	0.0833	-0.0132	0.0336	0.0499	-0.0125	0.0023	85.1776	233.8749	49.896
138	-0.0073	-0.0273	0.0465	-0.0077	-0.0261	-0.0017	-0.0249	0.0163	0.0355	-0.0098	-0.0826	-0.0932	0.0711	0.0676	-0.119	0.0532	-0.0119	-0.0129	-0.0413	-0.1095	-0.0346	84.9265	212.1737	55.3221
139	0.0865	0.121	0.0383	0.1684	0.0559	0.1344	0.0336	0.0279	0.0071	0.0924	-0.0761	-0.0952	0.0949	0.029	-0.0193	0.0716	-0.031	-0.0136	-0.0425	-0.0921	-0.04	84.4256	210.6485	77.8235
140	0.2258	-0.033	-0.2458	0.027	-0.0302	0.3212	0.0551	-0.0463	0.1086	-0.0213	0.0052	-0.0449	-0.0258	0.0106	-0.0339	0.0175	-0.0069	0.1939	0.4907	0.2608	0.5341	115.5375	90.4193	-19.6258
141	-0.0632	-0.0038	-0.0632	0.2595	0.1631	0.0591	0.0214	0.1031	0.1101	-0.0264	-0.0257	-0.0029	-0.0227	-0.0489	0.0089	0.0687	0.1513	0.1017	0.4702	0.1941	0.3226	115.5508	64.8372	-0.1451
142	-0.0839	0.1447	-0.1371	0.0141	-0.0525	-0.0567	0.0027	0.0748	0.0209	0.0269	0.0654	-0.0963	0.0305	0.0276	-0.0458	0.1992	0.116	-0.1749	0.4374	-0.0765	0.6091	115.0274	75.4352	30.0444
143	0.1768	-0.1581	0.0008	-0.176	-0	0.1287	-0.1527	0.0548	-0.0921	0.0684	-0.0504	-0.1103	-0.0097	-0.006	0.1281	0.1874	-0.2177	-0.0583	0.4075	-0.0166	0.4999	114.3565	107.5916	29.5638
144	-0.004	-0.0701	-0.0956	0.299	-0.1192	0.0412	-0.0193	-0.0291	0.0882	0.0281	-0.0354	-0.1806	0.055	0.0483	0.0569	0.1571	0.0495	0.0506	0.239	-0.0418	0.5591	114.8437	116.454	-0.9769
145	0.4159	-0.075	-0.1157	-0.0686	-0.0214	0.0204	-0.0222	0.0491	0.0501	-0.0077	0.0011	-0.0334	-0.0096	0.0358	0.0219	0.0657	-0.2192	0.193	0.3774	-0.1452	0.3978	115.8438	177.7557	27.75
146	-0.5226	0.1458	-0.0339	-0.012	0.0123	0.0861	0.0002	0.0048	0.0245	-0.009	0.0776	-0.128	-0.0018	0.0217	-0.0773	-0.0086	0.1306	0.0869	0.5113	-0.1455	0.7507	116.3624	146.0245	20.3912
147	0.7427	-0.1866	0.3017	0.0537	-0.1513	-0.0658	-0.0091	0.0459	-0.0232	-0.0109	-0.0227	-0.0602	0.0075	0.0086	0.0041	0.2064	0.4055	0.04	0.4177	0.0136	0.5338	115.6076	128.3656	47.2027
148	0.4576	-0.0089	-0.19	0.0103	-0.0976	-0.2431	-0.0032	-0.0454	-0.0961	0.0409	-0.0072	-0.1	-0.0266	0.0288	-0.0546	0.0972	-0.0676	-0.1317	0.2769	-0.183	0.4073	115.2053	178.8184	59.7483
149	-0.4923	0.1605	-0.1152	0.1691	0.0384	-0.0464	-0.0632	-0.0391	-0.0948	-0.0123	-0.0192	-0.0129	0.0178	0.1216	0.0556	0.2463	0.1774	-0.039	0.7571	0.0872	0.52	114.8538	-7.6503	36.8695
150	-0.6798	-0.0668	0.1408	0.5163	0.0718	0.2834	0.0169	-0.0757	-0.196	0.0913	-0.0656	-0.0137	-0.0739	0.0443	0.0235	0.0929	-0.2394	-0.0671	0.434	0.0657	0.4044	114.8597	44.2329	41.1645
151	0.2991	-0.0996	0.1382	0.0207	0.0133	-0.137	-0.068	-0.2512	-0.0869	-0.017	0.0417	-0.0552	-0.0276	0.1338	0.0086	0.2921	-0.1109	0.179	0.4429	-0.0319	0.458	115.4418	36.698	9.595
152	0.1286	0.1742	-0.3764	-0.13	0.1359	0.8814	-0.0277	-0.2774	0.0495	-0.081	-0.0323	-0.0832	0.0077	0.0252	0.0253	0.1759	0.0157	0.2892	0.4296	0.0146	0.4909	115.3998	4.7645	7.2144
153	-0.1208	0.009	0.0755	0.3839	0.0277	-0.0019	-0.0414	0.0018	0.0262	0.0379	-0.0637	0.0047	-0.0427	0.0661	0.0578	0.2901	-0.2326	-0.027	0.3578	-0.0101	0.1799	115.5104	253.8429	69.1006
154	-0.5749	0.1984	0.2549	-0.0511	-0.1851	0.1298	-0.0266	-0.0205	0.0546	0.0451	-0.0166	-0.0272	-0.0257	-0.08	0.0219	0.1291	0.0724	0.0809	0.2481	-0.0336	0.2099	116.1238	235.7357	42.7412
155	0.1233	0.2074	0.1915	-0.0339	0.0752	0.0324	-0.0658	0.0066	0.1284	0.0026	-0.0301	-0.0073	0.0491	0.1658	0.0574	0.1769	0.1242	0.1046	0.5621	0.0962	0.3576	115.9205	204.9721	52.2333
156	-0.0666	-0.0042	-0.0096	0.1313	-0.0917	-0.0155	-0.0024	0.0503	-0.0096	0.0052	0.0323	-0.0349	0.0371	0.0687	-0.0284	0.1663	0.215	-0.1665	0.473	-0.2719	0.319	114.818	204.1875	84.2038
157	0.1266	-0.1956	0.0476	0.1959	0.1198	0.1209	0.0161	-0.0014	-0.1179	0.044	0.1198	-0.0872	0.0401	0.0258	-0.1149	0.2566	0.1309	-0.1774	0.2054	-0.0942	0.6927	114.9444	148.8836	71.5715
158	-0.3406	-0.2007	-0.0449	-0.0731	0.0053	0.3373	-0.0039	0.0307	-0.0287	0.0114	0.0334	-0.0147	0.015	-0.0522	-0.0035	0.0979	-0.0693	-0.2301	0.2404	-0.0556	0.2839	114.5976	234.5815	95.2202
159	0.1363	0.1045	-0.0268	0.0576	0.0412	-0.0312	-0.0393	-0.006	-0.0817	-0.021	-0.0378	-0.0376	-0.0389	0.0337	0.0339	0.2255	-0.0924	-0.2251	0.2064	0.0997	0.529	114.5005	16.5763	57.1847
160	-0.0353	-0.1776	0.0172	0.3715	-0.1489	0.0564	0.0457	0.0673	0.0235	-0.1636	-0.0842	-0.1209	0.0918	0.0299	0.0291	0.0986	0.0517	0.0121	0.0616	0.0336	0.0684	91.6103	79.43	-16.2095
161	0.1902	0.0063	-0.1523	0.0662	-0.0895	0.4009	-0.0641	0.0623	-0.0089	-0.002	0.017	-0.0032	0.2912	0.0786	0.036	0.0935	-0.0064	-0.0211	-0.0081	0.0743	0.0795	91.3288	64.6504	10.5287
162	0.0061	-0.0965	0.1439	0.2373	0.0551	0.0207	0.0277	0.0002	-0.0452	0.1912	-0.0751	-0.0737	0.0423	0.1014	0.0752	0.0893	-0.0087	0.029	0.1327	0.0849	0.078	90.712	85.5136	32.823
163	1.0009	0.4285	-0.145	-0.1099	-0.4934	0.3045	0.0339	-0.1129	-0.0161	0.1878	-0.0313	-0.1148	-0.2295	0.065	-0.0072	0.0779	0.0073	-0.052	0.0069	-0.054	0.2328	90.3908	113.3113	19.9995
164	-0.2089	-0.2137	-0.3607	0.1993	0.1724	0.4884	0.0564	-0.0733	0.0319	-0.1853	-0.0173	-0.0697	-0.1271	0.1131	0.0132	0.1201	0.0611	0.0708	0.0403	0.0285	0.1712	91.059	109.4911	-10.2778
165	0.3638	0.1076	-0.1406	0.2955	0.0747	0.1634	-0.1012	-0.2372	0.0097	-0.064	0.0267	-0.1724	-0.0454	0.1551	-0.0171	0.0823	-0.0231	-0.0008	0.2191	-0.0571	0.0704	92.0335	167.6745	21.704
166	-0.1966	-0.0322	-0.0141	0.0876	0.0781	0.1301	0.0004	0.0343	0.0287	-0.1986	0.1227	-0.1941	0.1045	0.2011	-0.188	0.1043	-0.0054	-0.0551	-0.0475	-0.3251	0.2216	92.1287	137.3692	26.77
167	-0.244	-0.0072	0.1022	0.0515	0.0614	0.2407	0.1168	-0.0591	-0.0663	0.1117	-0.0443	-0.1232	0.1281	0.0873	-0.1092	0.0794	-0.0197	-0.0953	0.0736	-0.0173	0.2787	91.269	132.6088	56.7828
168	-0.0701	0.5931	0.5901	0.5408	0.6276	0.7493	0.0414	0.1689	-0.1745	0.1809	0.1666	-0.2274	-0.0416	0.2255	0.0374	0.0865	-0.0083	-0.0466	0.0849	-0.1622	-0.0915	90.908	160.0793	70.1791
169	-0.2479	0.2782	0.2511	0.4483	-0.238	-0.0131	-0.0776	-0.0418	-0.0808	0.1026	0.0752	-0.19	-0.1868	0.0979	-0.1094	0.0765	0.0153	0.0246	0.1182	-0.0709	0.0184	91.4699	181.731	48.6002
170	0.1936	0.0946	0.0251	0.1701	0.0393	0.0908	0.1104	0.0091	-0.1051	0.0509	-0.0864	-0.1405	-0.0223	0.0809	0.077	0.0757	-0.0299	-0.0379	0.0519	0.0936	0.087	90.6567	-1.8018	45.7558
171	0.0016	0.033	0.0058	0.4408	-0.3408	0.2937	0.0565	0.035	-0.0543	0.2929	-0.0454	0.0028	-0.0539	-0.0251	0.1501	0.0996	-0.0535	-0.0382	0.0788	-0.0104	0.0203	90.5607	27.6236	54.5489
172	0.0779	0.1795	-0.1031	0.176	-0.0674	0.05	0.0907	-0.1292	-0.0115	0.1053	0.081	-0.0607	-0.0773	0.1532	0.3065	0.048	0.0262	-0.0145	-0.1258	0.1731	-0.0587	91.0958	45.2046	29.4655
173	0.2611	0.1956	0.018	0.3624	0.3067	0.707	-0.1313	-0.0128	0.0547	-0.433	0.1361	-0.0362	-0.1021	0.0919	0.3034	0.1729	-0.0079	-0.0764	0.0214	-0.0107	-0.1048	91.3813	26.5149	5.2716
174	0.6457	-0.2894	0.149	-0.2544	0.0863	0.237	0.2116	0.123	0.0038	-0.1698	-0.087	0.0322	-0.0102	0.0818	-0.0281	0.1037	0.0216	0.0495	0.0129	0.0125	0.1363	91.2095	-2.4799	15.2988
175	0.009	-0.0044	0.0135	0.1751	0.0872	0.0941	0.0052	-0.0645	-0.0071	0.0724	0.0084	-0.109	-0.1225	0.0964	0.0949	0.0386	-0.027	0.0089	-0.297	-0.2373	-0.117	90.8261	243.7211	87.5184
176	0.2776	0.17	-0.5313	0.0926	-0.251	0.5682	0.043	-0.127	0.0531	0.0372	-0.031	-0.0451	-0.0808	0.1123	0.1303	0.0556	0.0086	0.0275	0.0241	0.0311	0.0122	91.8055	250.6694	57.7979
177	0.9469	-0.2891	0.4004	0.266	-0.0778	0.2874	0.0071	0.16	0.0958	-0.0371	-0.0253	-0.1358	0.1193	0.15	-0.1699	0.0604	0.0117	-0.0141	0.0474	-0.038	0.001	92.1917	224.5191	41.8448
178	0.1546	-0.0543	-0.1793	0.03	0.0268	0.313	-0.1275	0.0897	-0.028	-0.0514	-0.0531	-0.0816	0.2941	0.0528	-0.302	0.1134	-0.031	-0.0238	-0.0234	-0.0631	-0.0378	91.4864	201.5319	61.9543
179	0.6319	0.2807	0.1654	0.2666	0.2036	0.4855	0.0078	0.0611	-0.1044	0.0769	-0.0502	-0.1875	0.1913	0.0433	-0.2096	0.083	0.0017	-0.0089	0.0057	-0.0372	-0.1077	90.6135	213.0722	90.1677
180	0.4047	-0.4374	0.4254	0.2699	-0.3556	0.4099	0.1402	0.0192	-0.0805	-0.1838	-0.1238	0.0542	0.2007	0.0038	-0.0554	0.0856	0.0253	0.0053	0.0769	0.0197	0.0891	80.9842	79.7226	-22.5188
181	0.1197	0.0932	0.0475	0.0215	0.0575	0.0318	0.0359	-0.1672	0.1496	0.0375	-0.1412	0.1425	0.0056	-0.1383	0.1006	0.0564	-0.0196	-0.0632	0.148	-0.0736	0.1276	80.1299	157.9815	75.7075
182	0.1879	-0.0729	-0.5472	0.2709	0.0922	0.8299	-0.03	0.0033	-0.0123	-0.1041	-0.1587	-0.0163	0.0961	-0.1771	0.1204	0.0718	0.0298	0.0118	0.2349	0.0197	0.0084	81.7355	227.1242	36.0366
183	0.0176	-0.0546	-0.0228	0.1167	0.0018	-0.0628	-0.0567	0.0586	0.1071	0.1949	0.0515	-0.064	0.0297	0.0299	0.044	0.1637	0.0716	-0.0473	0.0256	0.143	0.1145	80.8599	58.8889	8.2365
184	0.0718	0.0496	-0.1021	-0.0144	-0.0487	0.0998	-0.0415	-0.0547	-0.1419	0.0584	-0.0611	-0.0819	-0.0478	0.0595	0.0711	0.0269	0.0117	-0.0402	0.1334	0.0637	0.1901	80.1202	81.5545	37.1845
185	0.1711	-0.0961	0.1194	-0.1885	0.0501	0.3144	0.0412	0.023	0.085	0.0477	-0.063	-0.128	-0.155	0.0437	0.0313	0.1283	0.0052	-0.0282	0.0743	-0.0109	0.2293	79.629	116.2644	24.859
186	0.1106	-0.1247	0.0682	0.0942	-0.1093	0.0489	0.0253	0.0508	-0.0223	-0.1603	-0.0269	0.0854	-0.0091	-0.0277	0.014	0.2745	0.1004	0.009	0.1104	-0.0093	0.1887	80.4527	115.1569	-11.9268
187	0.2182	-0.1033	-0.0925	0.3607	0.1686	0.1971	0.0723	0.0315	0.0653	-0.1442	0.0249	-0.1054	-0.0192	-0.0404	-0.009	0.1161	0.0222	0.0049	0.0567	-0.0882	0.1136	81.5298	172.3575	18.0056
188	0.1192	-0.3681	0.2522	0.4703	-0.2443	0.3122	0.0253	0.1358	0.1476	0.0072	-0.0126	-0.2356	0.0752	0.158	-0.0206	0.087	0.0392	-0.0252	0.1745	-0.0562	0.2731	81.7419	135.7364	20.7654
189	0.5732	-0.1269	0.0404	0.1999	-0.0386	0.0785	0.0899	0.0345	-0.1254	0.0497	-0.0818	-0.0472	0.0733	-0.0284	-0.0305	0.1886	0.0192	-0.0432	0.191	0.0118	0.1912	80.6985	126.6277	56.3993
190	0.1717	0.0567	-0.3717	-0.0525	0.1227	0.6021	-0.0127	-0.1455	0.0051	-0.0544	-0.0517	0.0417	-0.0347	0.166	-0.0195	0.1333	0.0601	0.0048	0.1677	-0.0515	0.0416	80.763	186.3506	52.0234
191	0.3363	-0.0241	0.1668	0.0292	-0.0498	0.1766	0.0569	-0.0039	-0.1764	0.0565	-0.0137	-0.0115	0.0169	0.0236	-0.03	0.0488	0.0174	-0.0238	0.0463	0.0576	0.1694	80.0596	-7.7234	46.4239
192	0.1487	-0.0619	0.3162	0.5452	0.4236	0.0954	0.1771	-0.0693	0.0115	0.3137	-0.0659	0.1023	-0.0139	0.0101	-0.0162	0.2084	-0.0504	0.0447	0.2785	0.0453	0.0498	79.8804	26.6327	60.1539
193	0.0372	0.0682	-0.1387	0.0449	-0.058	0.1386	0.1015	-0.0473	0.1434	-0.0049	0.0776	0.0491	-0.0957	0.0273	-0.0804	0.0202	-0.0847	0.0727	-0.0008	0.0091	0.1461	80.5183	50.5496	31.9914
194	0.0683	0.1699	-0.4164	1.2018	-0.4603	0.2645	-0.2049	-0.109	0.1035	-0.2543	0.1563	-0.008	0.2083	0.0178	0.053	0.2564	0.0516	-0.0311	0.1129	-0.0074	0.1323	80.9238	30.8212	1.0234
195	0.0193	0.204	-0.0233	0.3051	-0.1591	0.0918	-0.0119	0.0704	0.0243	-0.0885	0.0584	0.095	0.1554	0.1207	-0.0333	0.2142	-0.0056	-0.0231	0.1024	-0.0118	0.1352	80.6889	-5.1149	9.8319
196	0.3462	0.1015	0.1836	0.0446	-0.1322	0.1813	0.0216	0.0333	-0.1091	0.2724	-0.0512	-0.068	-0.2036	0.0558	-0.0107	0.144	-0.0721	0.004	0.0594	-0.0212	0.0527	80.0688	245.0486	92.9211
197	-0.0421	-0.0021	0.017	0.0693	0.0401	0.0474	0.0018	-0.0167	-0.0035	-0.1213	-0.0262	0.0299	0.0026	0.031	0.0234	0.1386	0.0896	0.0476	0.1109	0.0624	0.0738	81.271	256.6386	58.0948
198	0.038	-0.0612	0.3169	0.7472	0.659	1.2354	0.0094	-0.0523	0.0575	0.1912	-0.1703	0.0318	0.3876	-0.1517	0.0642	0.2095	-0.0157	-0.0589	0.068	-0.0399	0.0894	81.0157	197.1031	57.6293
199	0.352	0.4969	0.3309	0.308	0.2999	0.399	0.1903	-0.0169	-0.2801	0.2728	0.0161	-0.2794	0.0722	0.0426	-0.1182	0.1452	-0.0456	-0.022	0.0568	-0.0227	0.18	79.8616	207.964	92.7635
200	0.131	-0.321	0.0406	0.3087	-0.5072	0.7375	0.0358	0.0764	0.2128	-0.0336	-0.1131	-0.209	-0.173	-0.0915	0.0138	0.0952	0.0528	0.0541	0.0916	0.0567	0.132	99.4853	92.3235	-19.5451
201	0.0364	-0.1297	0.0579	0.2519	0.3939	0.4526	0.0422	0.1153	0.0232	-0.1433	0.0286	0.1238	-0.1963	0.1141	0.0635	0.0458	0.082	-0.0058	-0.0195	0.0358	0.134	99.6346	65.3549	-2.5078
202	0.3049	-0.2289	-0.1467	1.2486	0.234	0.2823	0.1302	-0.0546	-0.0046	-0.18	0.0815	-0.0855	0.0271	-0.1205	-0.0313	0.0639	-0.0032	0.0165	0.079	0.0853	0.0997	99.0383	73.36	28.3603
203	0.2391	0.1784	-0.0174	0.3617	-0.2416	0.1821	-0.072	-0.1024	-0.055	0.0335	-0.0806	-0.1222	-0.0622	-0.0337	-0.03	0.1066	-0.037	-0.0501	0.0284	-0.0407	0.0702	98.3508	105.2826	30.3946
204	-0.1988	-0.1096	-0.0899	0.7138	-0.0252	0.0841	-0.0335	-0.0315	0.1419	0.1749	0.0794	-0.1521	-0.145	0.0714	0.0936	0.1377	-0.1189	0.069	0.0194	0.033	0.2016	98.7664	116.9499	0.789
205	0.729	-0.314	-0.6205	0.7601	0.0081	0.382	0.1072	0.1364	0.1827	0.1886	0.0036	-0.1782	-0.1843	-0.0382	-0.0181	0.0956	-0.0317	-0	0.0413	-0.0161	0.1212	99.7824	178.4745	29.3836
206	0.3476	0.0756	-0.1457	-0.0223	-0.0056	0.283	0.056	0.0976	-0.181	-0.0934	0.0084	0.0056	-0.1288	0.1981	0.0484	0.126	-0.0545	0.0557	0.3105	-0.2065	0.2126	100.3863	148.1764	19.322
207	0.0374	0.2455	0.2991	0.5547	0.0962	0.0037	-0.0728	0.073	-0.1972	-0.1411	0.1644	-0.2092	-0.1381	0.0161	-0.0744	0.1443	0.0545	-0.0448	0.07	-0.1372	0.3707	99.6536	128.5784	44.5474
208	0.5114	-0.0314	0.5261	0.4538	-0.1633	0.6792	0.1522	-0.174	-0.1226	-0.0078	-0.0654	-0.2208	0.2162	-0.0915	-0.1509	0.0876	0.0124	-0.1084	0.1196	-0.0169	0.1788	98.8988	146.9245	70.4608
209	-0.0507	0.0104	-0.0282	-0.0351	0.157	0.2088	-0.1312	-0.0887	0.0452	0.0978	-0.0166	0.0629	0.1062	0.081	-0.1809	0.027	-0.0588	-0.0315	0.0183	-0.2087	0.1168	99.1708	177.4606	61.2458
210	0.373	-0.1238	-0.1165	0.8793	0.3525	0.064	-0.0659	-0.0946	-0.1652	-0.2432	-0.0484	-0.0639	-0.0971	0.0485	0.1131	0.1045	0.0439	0.02	0.0944	0.0601	0.1566	98.8996	-7.9252	34.2947
211	0.0956	0.0786	0.0394	0.1603	-0.1732	0.3328	-0.0085	-0.1774	-0.1134	-0.0826	-0.0293	-0.1267	0.0711	0.0251	-0.064	0.1401	-0.0332	-0.096	0.1619	0.0882	0.1033	98.5308	14.5221	56.899
212	0.2318	0.4749	-0.5557	0.5051	-0.1861	0.4673	0.0805	-0.1203	0.0114	0.1424	-0.0602	0.1715	-0.0483	0.1925	0.0152	0.115	-0.0401	0.0034	0.1458	0.0104	0.0832	98.8205	43.2615	42.6401
213	0.1183	0.1657	-0.0564	0.1631	0.1289	0.4295	0.0322	-0.0255	-0.0883	-0.1319	0.1441	-0.0362	-0.121	-0.1364	-0.0574	0.1665	-0.0704	0.0136	0.111	0.0135	0.027	99.4372	38.3347	11.1662
214	0.1103	0.0561	0.221	-0.124	0.0579	1.0891	-0.2038	0.1066	0.021	-0.2282	0.0006	-0.0671	-0.2175	0.0814	-0.1906	0.129	-0.0144	0.1156	-0.0093	-0.0731	0.0803	99.4203	6.7782	6.0477
215	0.084	-0.0623	-0.1695	0.3036	0.1164	0.5307	0.0223	-0.0011	0.038	0.1032	-0.1196	-0.0284	0.1705	-0.1285	0.0551	0.1403	-0.0129	-0.0002	0.145	-0.0478	0.0362	98.493	232.3987	94.6952
216	0.3097	0.2407	0.0917	0.4598	0.1259	1.0216	0.1503	-0.0112	0.1977	0.0758	0.1032	0.1232	-0.003	0.1229	-0.0736	0.1254	0.0012	0.0527	0.0348	0.0067	0.1266	99.449	253.6205	70.869
217	0.4388	-0.1136	-0.6538	0.3193	-0.0219	0.4989	0.0632	0.2762	0.0606	0.0242	-0.0533	-0.0575	-0.0224	-0.2257	-0.1416	0.0935	0.0158	0.0161	0.1786	0.0235	0.0632	100.1194	237.6735	43.2809
218	0.0689	-0.2883	0.2285	0.3028	0.3963	0.2916	0.0102	0.2101	0.0252	-0.235	-0.1262	0.0083	-0.1692	0.0114	-0.0606	0.1011	0.0364	0.0484	0.1502	-0.0694	0.0553	99.9284	206.4811	50.0462
219	0.1135	0.1382	0.0786	0.59	0.0863	0.2762	-0.0231	0.0445	-0.045	-0.0737	0.0811	-0.2348	-0.0437	-0.0174	-0.0206	0.0923	0.0163	0.0082	0.0293	-0.0159	0.0787	98.8756	203.1138	81.7364
220	0.1361	-0.1621	0.3347	0.3779	0.1691	0.1616	0.0449	-0.0099	0.0052	0.012	0.0101	-0.0166	0.0167	-0.0529	-0.0089	0.1265	0.0494	-0.0237	0.3411	-0.0716	0.1011	88.4728	66.6503	-15.8558
221	0.0383	-0.3153	-0.0942	0.3139	-0.121	0.0714	0.0492	0.0454	0.0582	0.0732	0.0084	0.0563	0.0333	0.0138	-0.0526	0.3807	0.0834	0.1252	0.2493	-0.0459	0.3017	87.0761	96.0545	39.888
222	-0.2801	-0.3148	-0.1648	0.3342	-0.2159	-0.0599	0.0258	-0.0093	0.0232	-0.0086	-0.0491	0.0114	-0.08	-0.0074	0.0182	0.41	-0.147	0.0733	-0.0101	-0.09	0.3621	86.9763	123.2584	12.1561
223	-0.0334	0.0535	-0.0402	0.0958	-0.1254	0.0878	-0.037	0.056	0.0243	-0.0833	0.087	0.0021	0.0358	-0.0331	-0.0284	0.3966	-0.1178	0.1766	0.4809	0.1366	0.2034	87.9689	105.1025	-22.388
224	0.3993	-0.0143	-0.3578	0.2313	-0.1042	0.0123	0.0314	0.1122	-0.0877	0.0571	0.0742	0.0411	-0.1895	-0.0968	-0.0645	0.3611	-0.0449	0.1296	0.6493	-0.0147	0.1071	88.9727	159.1025	12.321
225	-0.0045	-0.0475	0.0069	0.0356	-0.0224	0.0521	0.011	0.0231	-0.03	-0.0044	-0.0342	0.0362	-0.0074	-0.011	-0.0002	0.1205	0.0345	-0.0814	0.1915	-0.3393	0.3741	88.9575	125.4282	31.2926
226	0.2315	-0.1414	-0.1553	0.0171	0.0151	0.0156	-0.0051	-0.02	0.0413	-0.0001	0.0183	-0.0421	0.0034	-0.0032	-0.0145	0.3554	0.0686	-0.1865	0.6378	0.0372	0.5295	87.6427	133.7031	69.4155
227	-0.2565	-0.0728	-0.0866	0.2232	0.0386	-0.0065	-0.0437	-0.0127	0.1595	-0.033	0.0174	0.0206	0.0248	0.0243	0.0359	0.2313	-0.0525	-0.1016	0.2889	-0.0829	0.3019	87.3403	172.5676	72.7594
228	0.1343	0.1338	0.0474	-0.2195	0.0248	0.1639	0.0398	0.0231	-0.0032	0.0392	-0.026	-0.0075	-0.0093	-0.0126	-0.0135	0.3502	0.0089	0.1198	0.1953	0.144	0.3653	88.3685	188.662	37.8693
229	-0.0816	0.0051	0.0109	0.1188	-0.0434	0.1511	-0.0455	-0.0446	0.0204	0.0474	0.0664	-0.0144	-0.0347	-0.0216	-0.001	0.4752	0.2373	-0.0957	0.2733	0.0107	0.0617	87.2087	1.376	58.0669
230	0.0927	0.0301	0.1211	0.469	0.1805	-0.1492	0.0672	-0.0017	0.0117	0.0991	0.0082	-0.0052	-0.0019	0.0332	-0.0394	0.2608	-0.0281	-0.0003	0.2772	-0.1433	0.1783	87.3513	40.2694	55.6366
231	0.0086	-0.0288	0.0062	0.1529	0.3116	-0.0472	0.0492	-0.0098	0.0131	-0.1273	-0.0162	-0.0123	0.0395	0.0255	-0.0113	0.6349	-0.0149	0.163	0.1009	-0.1703	0.1402	88.0757	16.733	-2.8976
232	-0.1734	-0.0026	0.0376	0.272	0.1202	0.0275	-0.0022	-0.0191	0.0605	-0.1147	-0.0249	-0.0896	0.0216	-0.0296	0.0299	0.3594	0.1585	0.0239	0.1633	-0.0271	0.2063	87.6639	-13.241	22.1731
233	-0.2405	0.0797	0.3417	0.258	-0.1758	-0.0695	-0.0172	0.0758	0.0002	-0.1569	0.0044	0.0053	0.0345	0.0265	0.0048	0.4109	-0.2053	0.055	0.4848	0.0341	0.1688	88.8194	250.7893	45.0343
234	0.1394	-0.0361	-0.4204	0.3055	-0.4114	-1.2483	0.122	0.0098	-0.0007	0.0296	-0.0714	0.0254	-0.1525	-0.0263	-0.0302	0.3012	0.1185	0.0065	0.3344	-0.1524	0.0062	89.2243	212.4804	37.705
235	-0.114	0.0314	-0.0297	0.0148	0.1335	0.2548	-0.0445	-0.0268	-0.0173	-0.0489	-0.0344	0.0207	0.0262	0.0025	0.0404	0.4524	0.1458	0.1222	0.3136	0.0013	0.2278	87.7759	193.9711	71.9986
236	-0.2546	-0.2073	-0.8465	0.1563	0.3198	0.2028	0.1284	-0.1142	-0.0722	-0.0237	0.0447	-0.0014	-0.0194	0.0851	-0.0677	0.1659	-0.02	-0.0485	0.1306	-0.0254	0.0355	87.0202	220.1516	100.6151
237	0.1742	-0.0759	0.0513	-0.0331	-0.0362	0.116	-0.0241	-0.0026	0.0553	-0.0007	-0.0208	-0.0221	0.0292	0.0481	0.0204	0.1835	0.0601	0.0428	0.1858	0.1304	0.1973	88.0284	61.4299	22.79
238	-0.2311	-0.0356	-0.0161	0.0136	-0.1107	0.3074	0.0082	0.0294	-0.0002	-0.0322	0.0133	-0.0113	-0.0122	0.0117	-0.0027	0.2258	-0.1406	0.0412	0.0708	0.0419	0.141	87.9576	49.3762	17.5359
239	-0.3019	-0.1917	0.0553	0.2426	0.0852	0.084	0.0797	0.0038	0.0356	0.0108	0.0188	-0.0228	-0.0565	0.004	-0.051	0.2483	-0.0649	-0.0228	0.0996	0.001	0.3585	87.436	255.4471	82.9862
240	0.6007	0.4909	0.4097	1.5288	0.1672	0.2599	-0.022	0.0132	0.0147	-0.0176	0.0052	0.009	-0.0237	-0.0115	0.0063	0.8092	0.2348	0.1845	0.666	0.3711	0.6824	83.9792	64.0335	25.0891
241	1.4336	-1.7348	0.8433	3.3087	-0.9752	0.5907	-0.0235	-0.0141	-0.0055	0.0642	0.0204	0.0176	0.003	-0.0402	0.0028	0.7512	0.3539	-0.0468	0.4631	-0.1617	0.3	85.1443	155.3457	13.418
242	4.5227	0.381	6.6242	-1.2791	-0.8715	5.2381	-0.024	0.0032	0.0427	0.0345	0.0019	0.0141	-0.0707	-0.0343	0.0228	0.9196	0.129	-0.146	0.3911	0.1355	0.5691	85.3203	125.1953	34.9344
243	4.5503	4.5735	-0.0418	1.9997	1.8602	1.9745	0.023	0.0063	0.0279	-0.0123	-0.0097	0.0443	-0.0091	-0.0156	-0.0038	1.0165	0.1765	-0.0209	1.0985	-0.2166	1.0914	83.8233	137.2389	70.6323
244	0.8466	0.3033	1.2678	-0.3818	0.1404	3.7874	0.0056	0.0079	0.0102	0.0561	0.0124	0.018	-0.0439	-0.0101	-0.0107	0.7855	0.136	-0.0793	0.3238	0.0043	0.6676	83.7649	-12.7026	25.7883
245	0.219	-0.204	-0.3539	0.0041	0.1476	0.2379	0.0124	-0.0198	0.0288	-0.035	0.0122	-0.0127	-0.0089	-0.0023	-0.0159	0.6876	-0.0734	-0.0195	0.35	-0.0832	0.4916	83.2127	122.0568	8.6151
246	1.2011	-1.1674	0.8217	1.9899	-0.264	-0.2453	0.0091	-0.0091	-0.0111	0.018	-0.002	0.0002	0.0016	-0.0483	-0.0038	0.8378	-0.1773	-0.021	0.6581	0.0128	0.3236	84.8695	100.8121	-22.5849
247	0.894	-0.6475	-0.3491	0.4353	0.2914	0.3825	0.031	0.0076	0.0327	-0.0142	-0.0011	-0.0178	-0.0225	-0.0099	-0.0185	0.4379	0.1035	-0.0253	0.2973	0.1061	0.5391	84.6144	186.4686	34.7715
248	0.1979	0.2589	0.0383	0.3486	0.1546	-0.0164	0.0147	-0.0049	-0.0006	0.0214	-0.0107	0.0115	-0.0111	0.0159	-0.0018	0.4947	0.0818	-0.0584	0.4284	0.1196	0.2727	83.3753	5.0283	58.3714
249	0.3619	-0.5018	-0.3558	0.5049	0.2886	0.407	0.0349	0.0074	0.0171	-0.0524	0.0259	-0.0148	0.0726	-0.0269	-0.029	0.4491	-0.0173	-0.0313	0.2985	0.1298	0.4882	83.7997	46.8959	14.9854
250	1.3669	-0.6027	1.0443	1.2832	-0.2593	1.5229	-0.0074	-0.0206	0.0033	0.0267	-0.014	0.0231	0.0145	-0.0152	0.0125	0.908	-0.1637	-0.0651	0.5187	-0.1172	0.437	84.7863	13.1693	-0.9437
251	0.4689	-0.1084	-0.7821	0.1039	0.2798	1.0958	0.0088	0.0109	0.0038	-0.0671	-0.0186	0.0082	0.0148	-0.0197	0.0046	0.6034	0.1224	-0.032	0.4091	-0.0445	0.1097	83.306	255.685	79.4138
252	0.2523	-0.2009	-0.0074	0.1914	0.0238	-0.008	-0.0051	0.016	0.0008	0.0014	-0.0013	0.0091	-0.0025	0.0063	0.0025	0.3748	-0.2301	-0.1049	0.4799	0.0714	0.2666	85.0473	247.3676	43.5351
253	0.3619	-0.0785	0.2966	0.1482	-0.1193	0.2443	0.0117	-0.0243	0.0147	-0.022	0.0104	0.0058	0.0015	-0.0017	-0.0083	0.4081	-0.0987	0.2315	0.326	-0.1987	0.3529	85.2369	210.0228	40.486
254	1.9588	1.3783	-0.4799	1.6366	-0.2849	0.1446	0.0199	0.0237	0.0265	-0.0326	0.0203	0.0279	-0.0535	0.0099	-0.021	0.3005	0.0013	-0.0482	0.2666	-0.0327	0.0999	83.4266	223.9219	99.5269
255	0.4656	0.5545	-0.3589	0.8825	-0.4436	0.1276	0.013	0.0096	0.0034	-0.0357	-0.0222	0.0076	-0.0077	-0.0058	0.007	0.7828	-0.0316	-0.1751	0.3018	-0.0468	0.3777	82.8688	98.7323	37.95
256	1.5992	0.8778	-2.4163	0.6992	-1.4794	2.9414	-0.0082	0.0466	-0.0057	-0.0632	0.0042	-0.0002	-0.0017	0.0168	0.0009	0.7222	0.1377	-0.0388	0.4618	-0.1255	0.1352	83.0135	174.4728	70.0146
257	2.872	0.9204	-3.154	0.773	-1.4453	3.2158	-0.0218	0.0196	-0.0008	-0.0499	0.0071	0.0136	-0.0001	-0.0317	0.0143	0.6865	-0.0845	-0.15	0.4168	-0.2507	0.2742	83.1607	41.8685	52.3683
258	0.8187	0.6513	0.8228	0.6639	0.5874	0.4968	0.0243	-0.0045	0.0122	0.0125	0.0022	-0.0076	-0.0076	0.0023	-0.0102	0.6212	0.1218	0.1375	0.4742	-0.2138	0.2936	83.8483	196.0548	74.9342
259	0.1565	-0.0909	-0.118	0.1024	-0.0523	0.2756	0.0008	-0.0936	-0.1336	-0.0112	-0.061	-0.0599	0.1086	0.1096	0.1161	0.0685	0.0147	0.0548	0.0582	0.0553	0.0942	96.1533	82.3527	-18.8926
260	0.4856	-0.3478	-0.0989	0.5251	0.1944	0.2021	0.1017	-0.1385	0.0811	-0.1325	0.0192	-0.1427	0.0797	-0.1264	0.162	0.1068	0.0891	-0.0005	-0.0708	0.0048	0.1178	96.0114	62.9634	7.0645
261	0.168	0.1544	0.0605	0.0729	-0.1069	0.1612	0.1933	-0.0795	-0.0428	0.0399	-0.0822	0.0008	0.0566	-0.0187	-0.041	0.0465	0.0642	-0.0019	0.061	0.0809	0.1388	95.3125	81.6594	33.4972
262	0.3197	-0.1284	0.218	0.1733	-0.0821	0.1826	-0.1127	0.0288	0.1012	0.156	0.0338	-0.0628	-0.1721	0.0461	0.054	0.124	0.0037	-0.0193	0.091	-0.0256	0.1672	94.8734	112.776	24.0038
263	-0.0839	-0.1387	0.0258	-0.0478	0.0654	-0.0662	0.083	0.0333	0.0286	-0.033	-0.0483	-0.1433	-0.0764	-0.0237	0.0345	0.2006	-0.0403	0.0961	0.0873	0.0535	0.2552	95.4807	113.1272	-8.3468
264	-0.2285	-0.183	-0.4192	0.7337	0.2078	0.2056	0.0143	0.0833	-0.0423	-0.1654	-0.1801	-0.062	-0.0172	-0.1448	0.0923	0.116	-0.0372	0.0096	0.1492	-0.0276	0.1146	96.4954	171.7162	22.2083
265	0.1104	0.0625	-0.0182	0.0842	0.0823	0.0729	0.0663	0.0487	-0.1453	-0.1004	0.1022	-0.1475	0.0131	0.0616	-0.0052	0.0531	-0.0445	0.011	-0.0293	-0.2163	0.2307	96.8274	139.1402	23.2637
266	-0.0123	0.097	0.0971	0.2665	0.0136	0.1236	0.1455	-0.0034	-0.146	-0.0294	0.0234	-0.1448	0.1259	-0.0208	0.0068	0.1537	0.0545	-0.1167	0.0809	-0.0283	0.3418	95.9088	129.6455	54.2199
267	0.1998	0.0285	0.11	0.1338	0.1504	0.2869	0.0989	0.0006	-0.0289	0.0706	0.0501	-0.122	0.1763	-0.0092	-0.1426	0.1082	0.0153	-0.1142	0.0743	-0.0035	0.156	95.361	156.6145	72.2576
268	-0.0365	0.0668	-0.1619	0.3726	0.5139	0.5351	0.0667	-0.089	0.1098	-0.1507	0.0062	0.0145	-0.2309	0.0206	-0.0355	0.1257	0.0184	-0.0352	0.0993	-0.0661	0.1344	95.878	182.4031	52.5941
269	0.3064	-0.0139	-0.0427	0.3847	-0.0522	0.4681	0.0987	-0.0551	-0.0199	0.0687	-0.0418	-0.1275	0.1623	-0.0781	0.0112	0.128	0.007	-0.001	0.1168	0.0789	0.1322	95.2324	-5.1853	43.6699
270	0.0855	0.0475	0.1963	0.0643	-0.2238	0.202	-0.0155	-0.1579	-0.0214	0.1539	-0.0517	-0.0313	-0.14	0.0349	-0.0142	0.1223	-0.035	-0.0395	0.1366	0.069	0.0023	95.0601	24.4103	57.1182
271	-0.0817	0.3459	-0.1633	0.0161	0.2135	0.1674	0.0629	0.0837	-0.1225	-0.0819	0.1016	-0.0461	-0.0882	0.0863	0.0216	0.1023	-0.0377	-0.0466	0.0707	-0.0157	0.1007	95.5147	46.6299	33.2371
272	0.1832	-0.0066	-0.3604	0.2787	0.0336	0.2227	-0.0708	0.141	-0.1122	-0.2724	-0.0516	-0.1391	0.0441	-0.1166	0.0257	0.2232	-0.0791	0.0735	0.08	0.0199	0.0714	95.9588	30.4919	5.1496
273	0.4547	-0.5717	0.0534	-0.1414	-0.1858	0.1031	0.1206	0.0269	-0.1786	-0.1352	0.0691	-0.0106	0.0164	0.0588	0.0741	0.1224	-0.0782	0.1126	-0.0049	-0.0131	0.1218	95.8145	-1.3963	11.4815
274	0.3919	-0.2002	-0.0258	0.3474	0.1031	0.1199	-0.0229	-0.0366	0.1288	0.0793	0.0476	-0.017	0.0187	0.0659	0.0279	0.0953	0.0203	-0.0212	0.0524	-0.0101	0.0414	95.1613	241.7686	91.2331
275	0.4174	0.2731	-0.1028	0.3049	0.2312	0.2069	-0.0067	0.0997	0.0091	-0.1423	0.0565	-0.1562	-0.1804	-0.003	0.0216	0.1373	-0.0215	-0.0206	0.0822	0.0233	0.0308	96.2341	253.375	60.9391
276	0.4919	-0.012	-0.248	0.1174	-0.0132	0.5863	0.1305	0.2285	0.0247	-0.232	-0.0627	-0.0094	0.0226	-0.0487	-0.0191	0.0065	-0.0124	0.086	0.0545	0.024	-0.0179	96.7307	228.1268	40.4167
277	0.0473	-0.4592	0.2019	-0.0914	0.348	0.1367	0.1753	-0.0336	-0.0113	-0.0083	0.0477	-0.0836	0.1305	-0	0.2969	0.1038	0.0613	0.0524	0.0188	-0.0592	0.0942	96.1912	201.0412	58.1293
278	0.4254	-0.0337	-0.0632	0.3102	0.1359	0.3907	0.0557	-0.0621	0.013	0.04	-0.0333	-0.1082	0.2394	0.0526	-0.0288	0.0895	0.0233	-0.0081	0.0825	-0.0315	0.042	95.1625	209.234	89.4106

精密化 TLSグループ

ID	Refine-ID	Refine TLS-ID	Selection details
1	X-RAY DIFFRACTION	1	chain A and resid 1:12
2	X-RAY DIFFRACTION	2	chain B and resid 1:12
3	X-RAY DIFFRACTION	3	chain C and resid 1:12
4	X-RAY DIFFRACTION	4	chain D and resid 1:12
5	X-RAY DIFFRACTION	5	chain E and resid 1:12
6	X-RAY DIFFRACTION	6	chain F and resid 1:12
7	X-RAY DIFFRACTION	7	chain G and resid 1:12
8	X-RAY DIFFRACTION	8	chain H and resid 1:12
9	X-RAY DIFFRACTION	9	chain I and resid 1:12
10	X-RAY DIFFRACTION	10	chain J and resid 1:12
11	X-RAY DIFFRACTION	11	chain K and resid 1:12
12	X-RAY DIFFRACTION	12	chain L and resid 1:12
13	X-RAY DIFFRACTION	13	chain M and resid 1:12
14	X-RAY DIFFRACTION	14	chain N and resid 1:12
15	X-RAY DIFFRACTION	15	chain O and resid 1:12
16	X-RAY DIFFRACTION	16	chain P and resid 1:12
17	X-RAY DIFFRACTION	17	chain Q and resid 1:12
18	X-RAY DIFFRACTION	18	chain R and resid 1:12
19	X-RAY DIFFRACTION	19	chain S and resid 1:12
20	X-RAY DIFFRACTION	20	chain T and resid 1:12
21	X-RAY DIFFRACTION	21	chain A and resid 16:22
22	X-RAY DIFFRACTION	22	chain B and resid 16:22
23	X-RAY DIFFRACTION	23	chain C and resid 16:22
24	X-RAY DIFFRACTION	24	chain D and resid 16:22
25	X-RAY DIFFRACTION	25	chain E and resid 16:22
26	X-RAY DIFFRACTION	26	chain F and resid 16:22
27	X-RAY DIFFRACTION	27	chain G and resid 16:22
28	X-RAY DIFFRACTION	28	chain H and resid 16:22
29	X-RAY DIFFRACTION	29	chain I and resid 16:22
30	X-RAY DIFFRACTION	30	chain J and resid 16:22
31	X-RAY DIFFRACTION	31	chain K and resid 16:22
32	X-RAY DIFFRACTION	32	chain L and resid 16:22
33	X-RAY DIFFRACTION	33	chain M and resid 16:22
34	X-RAY DIFFRACTION	34	chain N and resid 16:22
35	X-RAY DIFFRACTION	35	chain O and resid 16:22
36	X-RAY DIFFRACTION	36	chain P and resid 16:22
37	X-RAY DIFFRACTION	37	chain Q and resid 16:22
38	X-RAY DIFFRACTION	38	chain R and resid 16:22
39	X-RAY DIFFRACTION	39	chain S and resid 16:22
40	X-RAY DIFFRACTION	40	chain T and resid 16:22
41	X-RAY DIFFRACTION	41	chain A and resid 26:60
42	X-RAY DIFFRACTION	42	chain B and resid 26:60
43	X-RAY DIFFRACTION	43	chain C and resid 26:60
44	X-RAY DIFFRACTION	44	chain D and resid 26:60
45	X-RAY DIFFRACTION	45	chain E and resid 26:60
46	X-RAY DIFFRACTION	46	chain F and resid 26:60
47	X-RAY DIFFRACTION	47	chain G and resid 26:60
48	X-RAY DIFFRACTION	48	chain H and resid 26:60
49	X-RAY DIFFRACTION	49	chain I and resid 26:60
50	X-RAY DIFFRACTION	50	chain J and resid 26:60
51	X-RAY DIFFRACTION	51	chain K and resid 26:60
52	X-RAY DIFFRACTION	52	chain L and resid 26:60
53	X-RAY DIFFRACTION	53	chain M and resid 26:60
54	X-RAY DIFFRACTION	54	chain N and resid 26:60
55	X-RAY DIFFRACTION	55	chain O and resid 26:60
56	X-RAY DIFFRACTION	56	chain P and resid 26:60
57	X-RAY DIFFRACTION	57	chain Q and resid 26:60
58	X-RAY DIFFRACTION	58	chain R and resid 26:60
59	X-RAY DIFFRACTION	59	chain S and resid 26:60
60	X-RAY DIFFRACTION	60	chain T and resid 26:60
61	X-RAY DIFFRACTION	61	chain A and resid 61
62	X-RAY DIFFRACTION	62	chain B and resid 61
63	X-RAY DIFFRACTION	63	chain C and resid 61
64	X-RAY DIFFRACTION	64	chain D and resid 61
65	X-RAY DIFFRACTION	65	chain E and resid 61
66	X-RAY DIFFRACTION	66	chain F and resid 61
67	X-RAY DIFFRACTION	67	chain G and resid 61
68	X-RAY DIFFRACTION	68	chain H and resid 61
69	X-RAY DIFFRACTION	69	chain I and resid 61
70	X-RAY DIFFRACTION	70	chain J and resid 61
71	X-RAY DIFFRACTION	71	chain K and resid 61
72	X-RAY DIFFRACTION	72	chain L and resid 61
73	X-RAY DIFFRACTION	73	chain M and resid 61
74	X-RAY DIFFRACTION	74	chain N and resid 61
75	X-RAY DIFFRACTION	75	chain O and resid 61
76	X-RAY DIFFRACTION	76	chain Q and resid 61
77	X-RAY DIFFRACTION	77	chain S and resid 61
78	X-RAY DIFFRACTION	78	chain T and resid 61
79	X-RAY DIFFRACTION	79	chain P and resid 61
80	X-RAY DIFFRACTION	80	chain R and resid 61
81	X-RAY DIFFRACTION	81	chain A and resid 62:67
82	X-RAY DIFFRACTION	82	chain B and resid 62:67
83	X-RAY DIFFRACTION	83	chain C and resid 62:67
84	X-RAY DIFFRACTION	84	chain D and resid 62:67
85	X-RAY DIFFRACTION	85	chain E and resid 62:67
86	X-RAY DIFFRACTION	86	chain F and resid 62:67
87	X-RAY DIFFRACTION	87	chain G and resid 62:67
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