SHEET DETERMINATION METHOD: DSSP THE SHEETS PRESENTED AS "EB" IN EACH CHAIN ON SHEET RECORDS BELOW ... SHEET DETERMINATION METHOD: DSSP THE SHEETS PRESENTED AS "EB" IN EACH CHAIN ON SHEET RECORDS BELOW IS ACTUALLY AN 6-STRANDED BARREL THIS IS REPRESENTED BY A 7-STRANDED SHEET IN WHICH THE FIRST AND LAST STRANDS ARE IDENTICAL. THE SHEET STRUCTURE OF THIS MOLECULE IS BIFURCATED. IN ORDER TO REPRESENT THIS FEATURE IN THE SHEET RECORDS BELOW, TWO SHEETS ARE DEFINED.
Resolution: 1.8→25 Å / Cor.coef. Fo:Fc: 0.912 / Cor.coef. Fo:Fc free: 0.865 / SU B: 2.69 / SU ML: 0.087 / Cross valid method: THROUGHOUT / ESU R: 0.125 / ESU R Free: 0.126 / Stereochemistry target values: MAXIMUM LIKELIHOOD Details: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS. REDIDUES 1 AND 2 OF CHAIN I ARE DISORDED THE CRYSTAL PRESENTED A HEMIHEDRAL TWIN (TWINNING FRACTION 0.5, TWINNING OPERATION -H -K L)
Rfactor
Num. reflection
% reflection
Selection details
Rfree
0.241
1301
4.8 %
RANDOM
Rwork
0.198
-
-
-
obs
0.2
25885
91 %
-
Solvent computation
Ion probe radii: 0.8 Å / Shrinkage radii: 0.8 Å / VDW probe radii: 1.4 Å / Solvent model: BABINET MODEL WITH MASK