5M6U
HUMAN PI3KDELTA IN COMPLEX WITH LASW1579
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2011-03-24 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9999 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 92.493, 113.212, 144.321 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 89.080 - 2.850 |
R-factor | 0.2569 |
Rwork | 0.256 |
R-free | 0.30890 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2wxr |
RMSD bond length | 0.009 |
RMSD bond angle | 1.055 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 89.080 | 3.000 |
High resolution limit [Å] | 2.850 | 2.850 |
Rmerge | 0.040 | 0.700 |
Number of reflections | 36112 | |
<I/σ(I)> | 7.7 | 1.1 |
Completeness [%] | 99.8 | 99.1 |
Redundancy | 6.5 | 6.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | NULL |