3SQO
PCSK9 J16 Fab complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 5.0.2 |
Synchrotron site | ALS |
Beamline | 5.0.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-11-08 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 1.0 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 81.921, 70.981, 109.156 |
Unit cell angles | 90.00, 95.90, 90.00 |
Refinement procedure
Resolution | 30.000 - 2.700 |
R-factor | 0.2261 |
Rwork | 0.223 |
R-free | 0.28280 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.062 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER (1.3.3) |
Refinement software | REFMAC |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 40.000 | 40.000 | 2.740 |
High resolution limit [Å] | 2.650 | 5.700 | 2.650 |
Rmerge | 0.119 | 0.048 | 0.472 |
Number of reflections | 35342 | ||
<I/σ(I)> | 10.2 | 15.3 | |
Completeness [%] | 94.7 | 98.1 | 73.5 |
Redundancy | 2.9 | 3.1 | 1.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.2 | 298 | 7% PEG 10000, 100 mM Hepes pH 7.2, VAPOR DIFFUSION, HANGING DROP, temperature 298K |